Development of a novel electron source linear ion trap/time-of-flight hybrid tandem mass spectrometer

被引:0
作者
Jiang, Zong-Yao [1 ,2 ]
Pan, Xin-Yuan [1 ,2 ]
Jia, Bin [2 ,3 ]
Xu, Guo-Bin [2 ,3 ]
Zhou, Zhen [1 ]
Yang, Peng-Yuan [2 ,3 ]
机构
[1] School of Environmental and Chemical Engineering, Shanghai University
[2] Novel Scientific Instrument Engineering Centre (MOE), Fudan University
[3] Department of Chemistry, Fudan University
关键词
Electron ionization (EI) source; Linear ion trap (LIT); Time of flight (TOF) analyzer;
D O I
10.7538/zpxb.2013.34.04.0193
中图分类号
学科分类号
摘要
This work introduces a novel electron source linear ion trap/time-of-flight hybrid tandem mass spectrometer. The system combine advantages of linear ion trap (LIT) and time-of-f light (TOF) mass spectrometry and it feathers good qualitative abilities. Standard sample of PFTBA, carbon tetrachloride and acetone is used to test the performances. The basic functions including ion trapping, isolation, collision induced dissociation (CID) and LIT-TOF interface has been proved to be excellent. Ion isolation and CID experiment of PFTBA fragment ion are demonstrated. Precise isotope ions isolation experiments shows the good selectivity performance of LIT. The EI LIT-TOF established in our laboratory can be applied to the fields of study the structure and chemical characters of volatile organic compounds (VOCs).
引用
收藏
页码:193 / 201
页数:8
相关论文
共 33 条
  • [1] Zhu J., Ji O., Design of a three-dimensional quadrupole ion trap, Analytical Instruments, 4, pp. 22-26, (1998)
  • [2] Hang W., Yang P., Wang X., Et al., Designation of pulsed Ion trap, Journal of Chinese Mass Spectrometry Society, 15, 1, pp. 23-28, (1993)
  • [3] Chen H., Li M., Fei Q., Et al., Mass calibration of miniaturized ion trap, Chinese Journal of Analytical Chemistry, 33, 10, pp. 1505-1508, (2005)
  • [4] Chen L., Huang R., Zhu H., Et al., Development of a radio-frequency ion trap mass spectrometer with external plasma source, Analytical Instruments, 3, pp. 8-11, (1997)
  • [5] Zhou C., Shi J., Feng Y., Et al., Establishment and study of ITD mass spectral data base, Research of Environmental Sciences, 7, 2, pp. 7-12, (1994)
  • [6] Yu J., Wen L., Li X., Et al., Development of an ion trap based gas chromatography mass spectrometry and its application, Chi-nese Journal of Scientific Instrument, 33, 9, pp. 2108-2114, (2012)
  • [7] Li X., Jiang G., Ding L., Et al., De-sign and performance of digital rectilinear ion trap mass spectrometer, Chinese Journal of Analytical Chemistry, 37, 9, pp. 1397-1402, (2009)
  • [8] Bai C., Sun Q., Gu C., Et al., Modeling and simulation of mass spectrum of rectangular ion trap, Chinese Journal of Vacuum Science and Technology, 30, 6, pp. 571-576, (2010)
  • [9] Hager J.W., A new linear ion trap mass spectrometer, Rapid Communications in Mass Spectrometry, 16, 6, pp. 512-526, (2002)
  • [10] Douglas D.J., Frank A.J., Mao D., Linear ion traps in mass spectrometry, Mass Spectrometry Reviews, 24, 1, pp. 1-29, (2005)