Influence of impulse frequency on anti-oxidation property of C-AlPO4 coating prepared by pulsed arc discharge deposition

被引:0
作者
Luo, Xiangdong [1 ,2 ]
Huang, Jianfeng [2 ]
Yang, Liuqing [2 ]
Hao, Wei [2 ]
Cao, Liyun [2 ]
Fei, Jie [2 ]
Wang, Kaitong [2 ]
Zhang, Yongliang [2 ]
机构
[1] School of Resources and Environment, Shaanxi University of Science and Technology
[2] School of Materials Science and Engineering, Shaanxi University of Science and Technology, Xi'an 710021, Shaanxi
来源
Kuei Suan Jen Hsueh Pao/Journal of the Chinese Ceramic Society | 2013年 / 41卷 / 10期
关键词
Anti-; oxidation; Carbon/carbon composites; Cristobalite aluminum phosphate; Impulse frequency; Pulsed arc discharge deposition;
D O I
10.7521/j.issn.0454-5648.2013.10.22
中图分类号
学科分类号
摘要
A C-AlPO4 anti-oxidation coating was prepared on SiC pre-coated C/C composites by pulsed arc discharge deposition. The phase compositions, microstructures and anti-oxidation properties of the as-prepared coatings were characterized by X-ray diffraction, scanning electron microscopy and isothermal oxidation test. The influence of impulse frequency on the microstructure was investigated. Results show that the dense and homogeneous C-AlPO4 coating was achieved when the impulse frequency reaches 1 000 Hz. The as-prepared coatings exhibit excellent anti-oxidation property, which could effectively protect C/C composites from oxidation at 1 773 K in air for 120 h with a mass loss of 0.5%. The anti-oxidation capability decrease of the coating at 1 773 K is due to the generation of cross-holes in the coating, which leads to the failure of self-curing by the metaphosphate glass layer after long time of oxidation.
引用
收藏
页码:1453 / 1458
页数:5
相关论文
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