Preparation and characterization of hydroxyapatite-poly(vinyl alcohol) composites reinforced with cellulose nanocrystals

被引:0
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作者
机构
[1] MOE Key Laboratory of Wooden Material Science and Application, College of Materials Science and Technology, Beijing Forestry University, Beijing
[2] Beijing Key Laboratory of Wood Science and Engineering, College of Materials Science and Technology, Beijing Forestry University, Beijing
[3] MOE Engineering Research Center of Forestry Biomass Materials and Bioenergy, College of Materials Science and Technology, Beijing Forestry University, Beijing
[4] Guangxi Eco-engineering Vocational and Technical College, Liuzhou
来源
Zhang, Shuangbao | 1600年 / North Carolina State University卷 / 09期
关键词
Articular cartilage repair; Cellulose nanocrystals; HAp/PVA composite gels; Preparation and characterization; Reinforcement;
D O I
10.15376/biores.9.4.6087-6099
中图分类号
学科分类号
摘要
Hydroxyapatite/poly(vinyl alcohol) (Hap/PVA) composites have been proposed as a promising biomaterial for use in articular cartilage repair. In this study, HAp/PVA composite gels reinforced with cellulose nanocrystals (CNC) were prepared using the freeze/thaw method. The influence of CNC as a reinforcement on the structure of composite gels was investigated via Fourier transform infrared spectroscopy (FT-IR), X-ray powder diffraction (XRD), and scanning electron microscopy (SEM). The mechanical properties and thermal stability of the composite gels were also studied. The FT-IR and XRD results indicated that the HAp/PVA/CNC composite gels were formed by hydrogen bonding. SEM morphology showed that the CNC served as an enhancement phase that interpenetrated the network of the HAp/PVA composite gels. The tensile strength and tensile modulus of the composites improved with increasing dosage of CNC. The thermal stability measurements indicated that the thermal stability of the HAp/PVA composites was slightly improved with the addition of the CNC.
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页码:6087 / 6099
页数:12
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