Microstructure and properties of Ti-3Zr-2Sn-3Mo-25Nb alloy prepared by SPS method

被引:0
|
作者
Ma X.-Q. [1 ]
Yu Z.-T. [1 ]
Liu H.-Y. [1 ]
Niu J.-L. [1 ]
Yu S. [1 ]
He X.-J. [1 ]
机构
[1] Shaanxi Key Laboratory of Biomedical Metal Materials, Northwest Institute for Nonferrous Metal Research, Xi'an
基金
中国国家自然科学基金;
关键词
Mechanical property; Medical β titanium alloy; Microstructure; Prealloyed powder; Spark plasma sintering;
D O I
10.19476/j.ysxb.1004.0609.2019.01.09
中图分类号
学科分类号
摘要
A biomedical β-Ti alloy Ti-25Nb-3Zr-3Mo-2Sn (mass fraction, %) was fabricated by spark plasma sintering (SPS). The characteristics, morphology and mechanical properties of TLM prealloyed powder after solid solution and aging were investigated. The results show that TLM prealloyed power prepared by plasma rotating electrode process has good spherical shape and high internal density. The solidification microstructure is consisted by small dendritic and single crystal. The sintered and as-soluted microstructures of TLM alloy propared by SPS method are equiaxed β phase and α″ martensite. The as-soluted alloy exhibits good comprehensive mechanical preperties with yield strength of 500 MPa, tensile strength of 624 MPa, elongation of 40% and elastic modulus of 54.5 GPa. Ageing at 500 ℃ for 6 h, after a superior the alloy has good plasticity, tensile strength reaches up to 1015 MPa, and the elastic modulus is 84 GPa. © 2019, Science Press. All right reserved.
引用
收藏
页码:74 / 80
页数:6
相关论文
共 21 条
  • [1] Li Y.-H., Yang C., Zhao H.-D., Qu S.-G., Li X.-Q., Li Y.-Y., New developments of Ti-based alloys for biomedical applications, Materials, 7, 3, pp. 1709-1800, (2014)
  • [2] Niinomi M., Boehlert C.J., Titanium Alloys for Biomedical Applications, pp. 179-213, (2015)
  • [3] Duan Y.-G., Ding Y.-Q., Zhang L., Liu Y.-Z., Tang X.-L., Biocompatibility of Ti35Nb3Zr2Ta a new beta-titanium alloy as joint prosthesis material, Chinese Journal of Tissue Engineeing Research, 19, 34, pp. 5536-5541, (2015)
  • [4] Li J., Li S.-J., Bai Y., Hao Y.-L., Yang R., Electrochemical behavior of nanostructured Ti2448 alloy in artficial saliva at 37 ℃ with fluoride, The Chinese Jeournal of Nonferrous Metals, 23, pp. s316-s319, (2013)
  • [5] Breme H., Biehl V., Reger N., Gawalt E., Metallic biomaterials: introduction, Handbook of Biomaterial Properties, pp. 151-158, (2016)
  • [6] Yu Z.-T., Zhang M.-H., Tian Y.-X., Cheng J., Ma X.-Q., Liu H.-Y., Wang C., Designation and development of biomedical Ti alloys with finer biomechanical compatibility in long-term surgical implants, Frontiers of Materials Science, 8, 3, pp. 219-229, (2014)
  • [7] Yilmazer H., Niinomi M., Nakai M., Cho K., Hieda J., Mechanical properties of a medical β-type titanium alloy with specific microstructural evolution through high-pressure torsion, Materials Science and Engineering C, 33, pp. 2499-2507, (2013)
  • [8] Zhu Y.-F., Wang L.-Q., Wang M.-M., Superelastic and shape memory properties of TixNb3Zr2Ta alloys, Journal of the Mechanical Behavior of Biomedical Materials, 12, 8, pp. 151-159, (2012)
  • [9] Ma X.-Q., Yu Z.-T., Niu J.-L., Yu S., Cheng J., Effect of heat trreatment on superelasticity in Ti-3Zr-2Sn-3Mo-25Nbn alloy, Rare Metal Materials and Engineering, 45, 6, pp. 1588-1592, (2016)
  • [10] Ma X.-Q., Yu Z.-T., Niu J.-L., Yu S., Liu C.-C., Microstructure and properties of ultrafine grained TLM alloy ARB sheet, Rare Metal Materials and Engineering, 43, 9, pp. 152-155, (2014)