Optimization of conditions for fabrication of a ceramic component through gel-casting technique

被引:0
作者
Dash, Rupashree [1 ,3 ]
Dash, Sukalyan [1 ]
Besra, Laxmidhar [2 ]
机构
[1] Veer Surendra Sai Univ Technol, Dept Chem, Burla 768018, Orissa, India
[2] CSIRInst Minerals & Mat Technol, Dept Mat Chem, Bhubaneswar 751013, Orissa, India
[3] Technol Bhavan, Dept Sci & Technol, New Mehrauli Rd, New Delhi 110016, Delhi, India
关键词
Alumina suspension; Ceramic; Darvan; 821A; Dispersant; Gel casting; ALUMINA; DISPERSION; BEHAVIOR;
D O I
10.56042/ijct.v31i5.10279
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
Gel-casting technique has been used for the production of alumina ceramic component. It is an attractive novel ceramic forming process for making high quality complex shaped ceramic part. The optimization of the alumina loading, pH, dispersant and catalyst amount has been successfully carried out for fabrication of high strength alumina component. A high green strength of alumina component is fabricated with 55 volume% slurry, for which 220 g of alumina powder, Darvan 821A (1.0 mg/g of alumina), N-(hydroxymethyl) acrylamide, 10 wt% initiator ammonium persulfate and 10 wt% catalyst tetra-methylethylenediamine). After slurry preparation, casting and subsequent drying is done by slow heating. The green body and the component obtained after binder burn out have been characterized through scanning electron microscope and X-ray diffraction techniques.
引用
收藏
页码:722 / 728
页数:7
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