Feasibility of laser induced breakdown spectroscopy for quantification of zirconium in nuclear streams

被引：0
|
作者：
Kumar, Satendra [1 ,2 ]
Maji, S. [1 ]
Sundararajan, K. [1 ,2 ]
机构：
[1] Indira Gandhi Ctr Atom Res, Analyt Chem & Spect Div, Kalpakkam 603102, India
[2] Homi Bhabha Natl Inst, Training Sch Complex, Mumbai 400094, India
来源：
JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY | 2024年
关键词：
LIBS; Zirconium; Nuclear; Quantification analysis; FUEL-CYCLE; QUANTITATIVE-ANALYSIS; METAL-IONS; WATER; CHROMIUM; FABRICATION; TECHNOLOGY; CHALLENGES; THORIUM; URANIUM;
D O I：
10.1007/s10967-024-09763-5
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Laser induced breakdown spectroscopy is explored for the estimation of Zr in metallic fuel and pyrochemical reprocessing stream using filter paper as a sample substrate. Zr(II) emission line at 339.20 nm has been identified and used for its quantitative determination. Calibration curves are obtained after normalizing the intensity of Zr to C/Y emission lines as an internal standard, to get better linearity. Analytical capability of LIBS for Zr estimation is tested by comparing the measured value with ICP-OES in simulated samples. Good agreement between the measured values confirms the ability of LIBS application in nuclear streams.
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页数：8
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