Sourcing and reducing sample environment background in low-temperature high-pressure neutron scattering experiments

被引:0
|
作者
Ma, Zhanwen [1 ]
Lass, Jakob [1 ]
Mazzone, Daniel [1 ]
Simutis, Gediminas [1 ]
Thursam, Sascha [1 ]
Fennell, Tom [1 ]
Pomjakushina, Ekaterina [1 ]
Bartkowiak, Marek [1 ]
Nikitin, Stanislav [1 ]
Bertelsen, Mads [2 ]
Willendrup, Peter [2 ,3 ,4 ]
Filges, Uwe [1 ]
Klauser, Christine [1 ]
机构
[1] Paul Scherrer Inst, CH-5232 Villigen, Switzerland
[2] European Spallat Source ERIC, Data Management & Software Ctr, Asmussens Alle 305, DK-2800 Lyngby, Denmark
[3] European Spallat Source ERIC, POB 176, Lund, Sweden
[4] Tech Univ Denmark, DK-2800 Lyngby, Denmark
关键词
RADIAL COLLIMATOR;
D O I
10.1016/j.nima.2024.169634
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Neutron scattering in high-pressure environments offers unique opportunities to measure the physical properties of matter but faces challenges due to low signal intensity and high background noise. In this study, Monte Carlo simulations were employed to identify background sources in low-temperature and high-pressure sample environments at the SINQ instrument CAMEA. Simulation results suggest that the piston pressure cell (PC) contributes significantly to the background noise in neutron scattering experiments. To counter this background, a compact radial neutron collimator was developed to reduce background in the sample environment, and its performance was evaluated experimentally. Measurements show that the collimator reduces the background generated by the PC effectively, especially for low q. Noise from the collimator was observed, and strategies to address this issue were discussed.
引用
收藏
页数:8
相关论文
共 50 条
  • [1] A sapphire cell for high-pressure, low-temperature neutron-scattering experiments on gas hydrates
    Rondinone, AJ
    Jones, CY
    Marshall, SL
    Chakoumakos, BC
    Rawn, CJ
    Lara-Curzio, E
    CANADIAN JOURNAL OF PHYSICS, 2003, 81 (1-2) : 381 - 385
  • [2] APPARATUS FOR HIGH-PRESSURE, LOW-TEMPERATURE, NEUTRON-SCATTERING MEASUREMENTS
    KLEB, R
    COPLEY, JRD
    REVIEW OF SCIENTIFIC INSTRUMENTS, 1975, 46 (09): : 1190 - 1192
  • [3] APPARATUS FOR HIGH-PRESSURE AND LOW-TEMPERATURE EXPERIMENTS
    GOLOPENTIA, DA
    RUOFF, AL
    REVIEW OF SCIENTIFIC INSTRUMENTS, 1981, 52 (02): : 235 - 238
  • [4] Cryogen free low temperature sample environment for neutron scattering experiments
    Kirichek, O.
    Evans, B. E.
    Down, R. B. E.
    Bowden, Z. A.
    25TH INTERNATIONAL CONFERENCE ON LOW TEMPERATURE PHYSICS (LT25), PART 1: CRYOGENIC TECHNOLOGIES AND APPLICATIONS, 2009, 150
  • [5] LOW-TEMPERATURE, HIGH-PRESSURE APPARATUS FOR NMR EXPERIMENTS
    VANDERPUTTEN, D
    PRINS, KO
    TRAPPENIERS, NJ
    REVIEW OF SCIENTIFIC INSTRUMENTS, 1985, 56 (04): : 603 - 606
  • [6] High-pressure/low-temperature neutron scattering of gas inclusion compounds: Progress and prospects
    Zhao, Yusheng
    Xu, Hongwu
    Daemen, Luke L.
    Lokshin, Konstantin
    Tait, Kimberly T.
    Mao, Wendy L.
    Luo, Junhua
    Currier, Robert P.
    Hickmott, Donald D.
    PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA, 2007, 104 (14) : 5727 - 5731
  • [7] SMALL SIZED NMR CELL FOR HIGH-PRESSURE LOW-TEMPERATURE EXPERIMENTS
    TROKINER, A
    DAHAN, N
    THEVENEAU, H
    PAPON, P
    REVIEW OF SCIENTIFIC INSTRUMENTS, 1984, 55 (10): : 1616 - 1619
  • [8] Characterising the sample environment in multianvil high-pressure experiments
    Rubie, DC
    PHASE TRANSITIONS, 1999, 68 (03) : 431 - 451
  • [9] Characterizing the sample environment in multianvil high-pressure experiments
    Bayerisches Geoinstitut, Universität Bayreuth, D-95440 Bayreuth, Germany
    Phase Transitions, 3 (431-451):
  • [10] A high-temperature high-pressure gas-handling cell for neutron scattering experiments
    Bailey, IF
    Done, R
    Dreyer, JW
    Gray, EM
    HIGH PRESSURE RESEARCH, 2004, 24 (02) : 309 - 315