[1] Inst Tecnol Agr Castilla & Leon, Consejeria Agr & Ganaderia, Ctra Burgos Km 119, Finca Zamaduenas, Valladolid 47071, Spain
[2] Univ Valladolid, Area Tecnol Alimentos, ETS Ingn Agr, Campus Yutera,Avda Madrid 50, Palencia 34004, Spain
[3] Univ Alcala, Dept Fis & Matemat, Campus Univ,Km 33-600, Alcala De Henares 28805, Spain
[4] Pago Carraovejas State Winery, Camino Carraovejas S-N, Valladolid 47300, Spain