Development of analysis method for m-xylenediamine as aldehyde scavenger using HPLC-PDA

被引:0
|
作者
Shim, Ji-Won [1 ]
Kim, Sun-Hae [1 ]
Shin, Han-Seung [2 ]
Shin, Jae-Wook [1 ]
机构
[1] Korea Adv Food Res Inst, 50 Botdeul Ro, Uiwang Si 16001, Gyeonggi Do, South Korea
[2] Dongguk Univ Seoul, Dept Food Sci & Biotechnol, 32 Dongguk Ro, Goyang Si 10326, Gyeonggi Do, South Korea
关键词
Smart packaging; Active packaging; m-xylenediamine; Analytical method; Method validation; MIGRATION; ACETALDEHYDE;
D O I
10.1007/s10068-024-01646-5
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
The objective of this study was to develop an analytical method for m-xylenediamine (m-XDA), an aldehyde scavenger, in various food simulants and food matrices. The analysis was performed using HPLC-UV (270 nm) with a Capcell pak MGII C18 column (4.6 x 250 mm, 5 mu m). The method validation encompassed evaluations of specificity, linearity, accuracy, precision, limit of detection (LOD), and limit of quantification (LOQ) across five food simulants and six food matrices. In the calibration curve range of 1-100 mu g/mL, excellent linearity was observed with R-2 >= 0.9992. The accuracy and precision were within the ranges of 86.4-98.6% and 0.7-2.9 relative standard deviation (RSD%), respectively. The LOD and LOQ were in the ranges of 0.26-0.56 mu g/mL and 0.79-1.71 mu g/mL, respectively. The significance lies in the development of analysis methods for each food matrix, not only for smart packaging simulant analysis. This research makes it well-suited for smart packaging safety management.
引用
收藏
页码:95 / 102
页数:8
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