Experimental investigation using conventional and natural extractants for liquid-liquid extraction of glutaric acid

被引：5

作者：

Mohadikar, Pranay ^{[1
]}

Kumar, Anuj ^{[1
]}

Wasewar, Kailas ^{[1
]}

Shinde, Diwakar Z. ^{[1
]}

机构：

[1] Visvesvaraya Natl Inst Technol VNIT, Dept Chem Engn, Adv Separat & Analyt Lab, Nagpur 440010, India

来源：

CHEMICAL DATA COLLECTIONS | 2022年 / 37卷

关键词：

Glutaric acid; Liquid-liquid extraction; Conventional extractants; Natural extractants; Physicochemical properties; Subject area; Chemical engineering; Compounds; Rice bran oil; Cyclohexane; Sesame oil; Sodium hydroxide and oxalic acid; Data category; Liquid-liquid equilibrium data; Data acquisition format; Titration; Data type; Experimental and analyzed; Procedure; Liquid-liquid extraction of glutaric acid using; conventional and natural extractants and; titrated with freshly prepared sodium; hydroxide solution; Data accessibility; All the experimental data is tabulated in the article; N-BUTYL PHOSPHATE; DI-(2-ETHYLHEXYL) PHOSPHORIC-ACID; REACTIVE EXTRACTION; PROPIONIC-ACID; LACTIC-ACID; NICOTINIC-ACID; OCTYL AMINE; ALIQUAT; 336; SEPARATION; INTENSIFICATION;

D O I：

10.1016/j.cdc.2021.100790

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Glutaric acid finds major application in corrosion inhibitors, anti -scaling agents, pharmaceutical synthesis, etc. mainly as a polymer building block. However, production of glutaric acid is quite difficulty, necessitated research into viable options for glutaric acid recovery. The liquid -liquid extraction method has been employed to recover glutaric acid from aqueous phase using a variety of inert extractant (cyclohexane) and natural, non-toxic extractants (rice bran and sesame oil). The extraction efficiency (%E) and distribution coefficient (K-D) were calculated based on equilibrium data obtained at 298.15 +/- 1 K. The trend observed for the average distribution coefficient along with extraction efficiency respectively are as follows: rice bran oil (0.152, 12.48%) > Cyclohexane (0.075, 6.90%) > Sesame oil (0.037, 3.53%). The rice bran oil has the highest extraction efficiency, whereas sesame oil provided the lowest extraction efficiency.

引用

页数：6

共 43 条

[1] Effect of temperature on equilibria for physical and reactive extraction of protocatechuic acid
Antony, Fiona Mary
Wasewar, Kailas
[J]. HELIYON, 2020, 6 (05)
[2] Efficacy of tri-n-octylamine, tri-n-butyl phosphate and di-(2-ethylhexyl) phosphoric acid for reactive separation of protocatechuic acid
Antony, Fiona Mary
Wasewar, Kailas
De, Biswajit S.
[J]. SEPARATION SCIENCE AND TECHNOLOGY, 2019, 54 (18) : 3100 - 3114
[3] Reactive separation of protocatechuic acid using Tri-n-octyl amine and Di-(2-ethylhexyl) phosphoric acid in Methyl isobutyl ketone
Antony, Fiona Mary
Wasewar, Kailas L.
[J]. SEPARATION AND PURIFICATION TECHNOLOGY, 2018, 207 : 99 - 107
[4] Separation of Protocatechuic Acid Using Di-(2-ethylhexyl)phosphoric Acid in Isobutyl Acetate, Toluene, and Petroleum Ether
Antony, Fiona Mary
Wasewar, Kailas
[J]. JOURNAL OF CHEMICAL AND ENGINEERING DATA, 2018, 63 (03) : 587 - 597
[5] Stoichiometric and Spectroscopic Study of Reactive Extraction of Phenylacetic Acid with Tri-n-Butyl Phosphate
Athankar, K. K.
Wasewar, K. L.
Varma, M. N.
Shende, D. Z.
Uslu, H.
[J]. CHEMICAL AND BIOCHEMICAL ENGINEERING QUARTERLY, 2015, 29 (03) : 385 - 394
[6] Dandekar P., 2020, Chem. Data Collections, V30, P100564, DOI [DOI 10.1016/J.CDC.2020.100564, 10.1016/j.cdc.2020.100564]
[7] databridgemarketresearch, 2016, Market research report on Global and Chinese Glutaric acid Industry
[8] De B.S., 2018, Chem. Data Collect., V15-16, P244, DOI [10.1016/j.cdc.2018.07.001, DOI 10.1016/J.CDC.2018.07.001]
[9] Dean J.A., 1987, Handbook of Organic Chemistry, P8
[10] Selective extraction of glutaric acid from biological production systems using n-butanol
Han, Yeong-Hoon
Park, Ye-Lim
Yang, Soo-Yeon
Jung, Hye-Rim
Joo, Jeong Chan
Song, Bong-Keun
Lee, Sang Hyun
Park, Kyungmoon
Ahn, Jung-Oh
Yang, Yung-Hun
[J]. JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY, 2020, 82 : 98 - 104

← 1 2 3 4 5 →