In-situ observation of Ni-11.5 wt%Si eutectic microstructure evolution and exploration of strengthening mode of Ni-Ni3Si eutectic composites

被引:1
作者
Wu, Chongyang [1 ]
Cui, Chunjuan [1 ]
Liu, Wei [1 ]
Zhang, Kai [1 ]
Wang, Zhicong [1 ]
Zhao, Yanan [1 ]
Su, Haijun [2 ]
机构
[1] Xian Univ Architecture & Technol, Sch Met Engn, Xian 710055, Peoples R China
[2] Northwestern Polytech Univ, State Key Lab Solidificat Proc, Xian 710072, Peoples R China
关键词
Directional solidification; In-situ observation; Microstructure; Metastable phaseNi31Si12; Heat treatment; Fracture morphology;
D O I
10.1016/j.matchemphys.2024.129063
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Microstructure evolution of the Ni-11.5 wt%Si eutectic alloy during the melting and cooling process was elaborately examined using a high-temperature confocal laser scanning microscope (HT-CLSM). The thermal stability of the phase composition within the Ni-11.5 wt%Si eutectic alloy was thoroughly analyzed. The intricate mechanism governing the solidification of the Ni-11.5 wt%Si eutectic alloy, along with the formation of the metastable Ni31Si12 phase under varying cooling rates, was systematically investigated. Through in-depth in-situ observations, a welldefined heat treatment procedure was developed for Ni-Ni3Si eutectic composites. Remarkably, the metastable Ni31Si12 phase can completely transform into Ni3Si upon undergoing the prescribed heat treatment, yielding a refined lamellar structure. This structural refinement notably results in substantial enhancements in the compressive properties and fracture toughness of the Ni-Ni3Si eutectic composite at ambient temperatures.
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页数:13
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