Crystal structure and Hirshfeld surface analysis of 3-phenyl-1-{3-[(3-phenylquinoxalin-2-yl)oxy]propyl}-1,2-dihydroquinoxalin-2-one

被引：2

作者：

Abad, Nadeem ^{[1
,2
]}

Mague, Joel T. ^{[3
]}

Alsubari, Abdulsalam ^{[4
]}

Essassi, El Mokhtar ^{[5
]}

Alzahrani, Abdullah Yahya Abdullah ^{[6
]}

Ramli, Youssef ^{[1
,7
]}

机构：

[1] Mohammed V Univ, Fac Med & Pharm, Drug Sci Res Ctr, Lab Med Chem, Rabat, Morocco

[2] Mohammed V Univ, Lab Heterocycl Organ Chem, Fac Sci, Rabat, Morocco

[3] Tulane Univ, Dept Chem, New Orleans, LA 70118 USA

[4] 21 September Univ, Fac Clin Pharm, Lab Med Chem, Sanaa, Yemen

[5] Mohammed V Univ, Lab Heterocycl Organ Chem, Fac Sci, Rabat, Morocco

[6] King Khalid Univ, Fac Sci & Arts, Dept Chem, Mohail, Assir, Saudi Arabia

[7] Mohammed VI Ctr Res & Innovat CM6, Rabat 10000, Morocco

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2024年 / 80卷

关键词：

crystal structure; quinoxaline; alkylation; hydrogen bond; pi-stacking; Hirshfeld surface analysis;

D O I：

10.1107/S2056989024001518

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C31H24N4O2, the quinoxaline units are distinctly nonplanar and twisted end-to-end. In the crystal, C-H center dot center dot center dot O and C-H center dot center dot center dot N hydrogen bonds link the molecules into chains extending along the a-axis direction. The chains are linked through pi-stacking interactions between inversion-related quinoxaline moieties.

引用

页码：300 / +

页数：12

共 28 条

[11] Synthesis, crystal structure, hirshfeld surface analysis, DFT computations and molecular dynamics study of 2-(benzyloxy)-3-phenylquinoxaline [J].

Abad, Nadeem ;

Lgaz, Hassane ;

Atioglu, Zeliha ;

Akkurt, Mehmet ;

Mague, Joel T. ;

Ali, Ismat H. ;

Chung, Ill-Min ;

Salghi, Rachid ;

Essassi, El Mokhtar ;

Ramli, Youssef .

JOURNAL OF MOLECULAR STRUCTURE, 2020, 1221

[12] Crystal structure, Hirshfeld surface analysis and DFT study of 1-ethyl-3-phenyl-1,2-dihydro-quinoxalin-2-one [J].

Al Ati, Gamal ;

Chkirate, Karim ;

Mashrai, Ashraf ;

Mague, Joel T. ;

Ramli, Youssef ;

Achour, Redouane ;

Essassi, El Mokhtar .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2021, 77 :18-+

[13] 1-Allyl-3-phenylquinoxalin-2(1H)-one [J].

Benzeid, Hanane ;

Bouhfid, Rachid ;

Massip, Stephane ;

Leger, Jean Michel ;

Essassi, El Mokhtar .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O2990-U983

[14] 1-Benzyl-3-phenylquinoxalin-2(1H)-one [J].

Benzeid, Hanane ;

Saffon, Nathalie ;

Garrigues, Bernard ;

Essassi, El Mokhtar ;

Ng, Seik Weng .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :O2685-U219

[15] 1-Methyl-3-phenylquinoxalin-2(1H)-one [J].

Benzeid, Hanane ;

Essassi, El Mokhtar ;

Saffon, Nathalie ;

Garrigues, Bernard ;

Ng, Seik Weng .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :O2323-+

[16]

Brandenburg K., 2012, DIAMOND

[17]

Bruker, 2016, APEX3 and SAINT

[18] 3-{2-[(3-Phenylquinoxalin-2-yl)oxy]ethyl}-1,3-oxazolidin-2-one [J].

Daouda, Ballo ;

Brelot, Lydia ;

Doumbia, Mouhamadou Lamine ;

Essassi, El Mokhtar ;

Ng, Seik Weng .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O1235-U1450

[19] The Cambridge Structural Database [J].

Groom, Colin R. ;

Bruno, Ian J. ;

Lightfoot, Matthew P. ;

Ward, Suzanna C. .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2016, 72 :171-179

[20] Comparison of silver and molybdenum microfocus X-ray sources for single-crystal structure determination [J].

Krause, Lennard ;

Herbst-Irmer, Regine ;

Sheldrick, George M. ;

Stalke, Dietmar .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2015, 48 :3-10

← 1 2 3 →