Evolution of interfacial microstructure and oxides of CLAM steel by hot compression bonding

被引:0
|
作者
Bai, Yunfei [1 ,2 ]
Wang, Jianqiang [3 ,4 ]
Zhu, Gaofan [1 ,2 ]
Nagasaka, Takuya [5 ]
Shen, Jingjie [5 ]
Sun, Mingyue [3 ,4 ]
Huang, Qunying [1 ]
机构
[1] Chinese Acad Sci, Inst Nucl Energy Safety Technol, Hefei Inst Phys Sci, Hefei 230031, Anhui, Peoples R China
[2] Univ Sci & Technol China, Hefei 230026, Anhui, Peoples R China
[3] Chinese Acad Sci, Key Lab Nucl Mat & Safety Assessment, Inst Met Res, Shenyang 110016, Liaoning, Peoples R China
[4] Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Liaoning, Peoples R China
[5] Natl Inst Fus Sci, 322-6 Oroshi, Toki, Gifu 5095292, Japan
基金
中国国家自然科学基金;
关键词
Hot compression bonding; CLAM steel; Interfacial oxide; Interfacial grain boundary; Holding time; STAINLESS-STEEL; MECHANICAL-PROPERTIES; RECRYSTALLIZATION; MORPHOLOGY; OXIDATION; BEHAVIOR;
D O I
10.1016/j.matchar.2024.113848
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The development of the joining process is essential for the application of China low activation martensitic (CLAM) steel as the structural material for fusion reactors. In the present study, the hot compression bonding (HCB) for CLAM steel was carried out under different parameters. The effects of different strain rates, temperatures, strains and holding time on the evolution of interfacial microstructure and oxides were investigated. Compressed at 1000 degrees C with 5% deformation, some micron-size continuous oxides distributed along the flat interface. The interfacial oxides were broken and decomposed as the deformation increased to 20%, their average size was reduced to 400 nm. With the bonding temperature increasing, more interfacial grain boundaries (IGBs) could cross the original bonding interface and flat interface became wavy. Compressed at 1000 degrees C/20%, the interfacial oxides consisted of fcc-structured spinel MnCr 2 O 4 and enriched in Si and Ta oxides. The MnCr 2 O 4 oxides would decompose preferentially after 0.5 h holding treatment at 1100 degrees C. Only a small number of oxides rich in Si and Ta elements remained at the original bonding area after 2 h holding treatment. Compressed at 1100 degrees C/20%, the bonding interface was completely replaced by the migrated grains after 2 h holding treatment and no large-size oxides could be observed. Moreover, the tensile strength and elongation at room temperature of the joint were comparable to those of the base material.
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页数:12
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