Effect of fuel type and synthesis temperature on magnetic properties of ZnFe2O4 nanomaterials synthesized by sol-gel method

被引：1

作者：

Bayan, Ekaterina ^{[1
]}

Mokliak, Maria ^{[1
]}

Rusalev, Yury ^{[2
]}

Tolstunov, Mikhail ^{[1
,3
]}

机构：

[1] Southern Fed Univ, Chem Fac, Rostov Na Donu, Russia

[2] Southern Fed Univ, Smart Mat Res Inst, Rostov Na Donu, Russia

[3] Russian Acad Sci, Southern Sci Ctr, Rostov Na Donu, Russia

来源：

JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY | 2024年 / 111卷 / 03期

关键词：

ZnFe2O4; Ferrites; Sol-gel method; Fuel type; Magnetic properties; SPINEL ZNFE2O4; NANOPARTICLES; FERRITE; PHASE; NI;

D O I：

10.1007/s10971-024-06489-4

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

ZnFe2O4 nanomaterials were synthesized using the sol-gel method with different fuels: citric acid, tartaric acid, ascorbic acid and glucose monohydrate. The effects of organic fuel type and calcination temperature on the magnetic properties of zinc ferrite were studied. X-ray diffraction analysis, thermogravimetric analysis, differential scanning calorimetry, and transmission electron microscopy were used to investigate the process of zinc ferrite formation during the calcination of intermediate gel products, as well as to analyze the crystal structure and samples morphology. The formation of hematite and wurtzite secondary phases was confirmed for some materials, and the influence of heat treatment conditions on impurity formation was discussed. The particle size of zinc ferrite was 11-39 nm depending on the calcination temperature and selected fuel. According to data obtained using a vibrating sample magnetometer, the ZnFe2O4 nanoparticles exhibited ferrimagnetic behavior with saturation magnetization values of 1.92-15.61 emu/g. Changing the fuel type and the calcination temperature makes it possible to obtain ZnFe2O4 nanomaterials with specific magnetic properties.

引用

页码：783 / 793

页数：11

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