A method with ultra-high angular resolution for X-ray diffraction experiments

被引:1
|
作者
Zhang, X. M. [1 ]
Zheng, X. [2 ]
Li, X. L. [2 ]
Meng, F. Q. [1 ,3 ]
Yin, S. S. [4 ]
机构
[1] Inst Adv Sci Facil, Shenzhen 518107, Peoples R China
[2] Chinese Acad Sci, Shanghai Adv Res Inst, Shanghai 201204, Peoples R China
[3] Sun Yat Sen Univ, Guangzhou 510275, Peoples R China
[4] ShanghaiTech Univ, Shanghai 201210, Peoples R China
基金
中国国家自然科学基金;
关键词
deconvolution; super resolution; X-ray diffraction; crystal truncation rod; SPATIAL-RESOLUTION; DECONVOLUTION; ALGORITHM;
D O I
10.1107/S160057752300961X
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
X-ray diffraction measurements, the angular resolution has a detection limit due to the receiving size of the detector. In many cases this detection limit is too large and must be breached to obtain the desired information. A novel method is proposed here by making the detector simultaneously measuring and moving. Using the deconvolution algorithm to remove the convolution effect, the pixel size limitation is finally broken. The algorithm used is not a common one, and suppresses signals at high frequencies, ensuring the reliability of the peak shape after restoration. The feasibility of this method is verified by successfully measuring the crystal truncation rod signal of SrTiO3 single crystal, and the resolution is nearly ten times higher than that of a single pixel. Moreover, this method greatly reduces the noise and improves the signal-to-noise ratio.
引用
收藏
页码:35 / 41
页数:7
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