Synthesis and Crystal Structure of N-(Biphenyl-2-thiocarbamoyl)-4-(1,3-dichlorophenyl) Carboxamide

被引：0

作者：

AAMER SAEED ^{[1
]}

ULRICH FL?RKE

机构：

[1] Department of Chemistry, Quaid-I-Azam University

[2] Department Chemie, Fakult?t fur Naturwissenschaften, Universit?t Paderborn

来源：

结构化学 | 2015年 / 34卷 / 06期

关键词：

synthesis; crystal structure; N-(biphenyl-2-thiocarbamoyl)-4-(1; 3-dichlorophenyl);

D O I：

暂无

中图分类号：

O76 [晶体结构];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The synthesis of the title molecule was achieved by the reaction of 2,4-dichlorobenzoyl chloride with potassium thiocyanate in 1:1 molar ratio in dry acetonitrile to afford the corresponding isothiocyante in situ followed by the treatment with 2-aminobiphenyl. The structure of the target compound was established by elemental analysis, FTIR, 1H, 13 C NMR and mass spectroscopy and unequivocally confirmed by the crystallographic data. The title compound crystallizes in the monoclinic space group P21/n with a = 13.356(2), b = 7.0761(11), c = 20.539(3) , β = 105.723(4)°, V = 1868.5(5) 3 and Z = 4.

引用

页码：853 / 857

页数：5

共 12 条

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[5]

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