2-Hydroxy-N'-(5-hydroxy-2-nitrobenzylidene)-3-methylbenzohydrazide

被引：1

作者：

Zhu, Zhao-Fu ^{[1
]}

Shao, Li-Juen ^{[1
]}

Shen, Xi-Hai ^{[1
]}

机构：

[1] Hebei Normal Univ Sci & Technol, Dept Chem, Qinhuangdao 066600, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-to-parameter ratio = 13.7; mean σ(C-C) = 0.003 Å; R factor = 0.051; single-crystal X-ray study; T = 298 K; wR factor = 0.132;

D O I：

10.1107/S1600536812002437

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C 15H 13N 3O 5, was prepared by condensing 5-hydroxy-2-nitrobenzaldehyde and 2-hydroxy-3-methylbenzohydrazide in methanol. The two benzene rings make a dihedral angle of 3.9 (3)°. An intra-molecular O - H⋯O hydrogen bond is observed. The crystal structure is stabilized by intermolecular O - H⋯O and N - H⋯O hydrogen bonds, and C - H⋯O and π-π inter-actions [centroid-centroid distances = 3.5658 (17)-3.9287 (19) Å].

引用

页码：O559 / U1099

页数：8

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