2-Hydroxy-N'-(5-hydroxy-2-nitrobenzylidene)-3-methylbenzohydrazide

被引：1
作者：
Zhu, Zhao-Fu [1 ]
Shao, Li-Juen [1 ]
Shen, Xi-Hai [1 ]
机构：
[1] Hebei Normal Univ Sci & Technol, Dept Chem, Qinhuangdao 066600, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词：
data-to-parameter ratio = 13.7; mean σ(C-C) = 0.003 Å; R factor = 0.051; single-crystal X-ray study; T = 298 K; wR factor = 0.132;
D O I：
10.1107/S1600536812002437
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C 15H 13N 3O 5, was prepared by condensing 5-hydroxy-2-nitrobenzaldehyde and 2-hydroxy-3-methylbenzohydrazide in methanol. The two benzene rings make a dihedral angle of 3.9 (3)°. An intra-molecular O - H⋯O hydrogen bond is observed. The crystal structure is stabilized by intermolecular O - H⋯O and N - H⋯O hydrogen bonds, and C - H⋯O and π-π inter-actions [centroid-centroid distances = 3.5658 (17)-3.9287 (19) Å].
引用
收藏
页码：O559 / U1099
页数：8
相关论文
共 50 条
  • [21] (E)-4-Hydroxy-N'-(2-hydroxy-3,5-diiodobenzylidene)-3-methoxybenzohydrazide methanol monosolvate
    Li, Xiao-Yan
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O654 - U1754
  • [22] Methyl N-hydroxy-N-(2-methylphenyl)carbamate
    Zhang, Binbin
    Wang, Yifeng
    Dong, Kun
    Xu, Danqian
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O230 - +
  • [23] Diphenylboron chelate of an 3-hydroxy-N-(2-hydroxyalkyl)hydroxamic acid
    Kliegel, W
    Schumacher, U
    Patrick, BO
    Rettig, SJ
    Trotter, J
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2002, 58 : O1215 - O1217
  • [24] Diaquabis(4-hydroxy-5-nitropyridine-2-carboxylato-κ2N1,O2)copper(II)
    Shi, Fengjuan
    Deng, Jiguang
    Dai, Hongxing
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : M46 - +
  • [25] (E)-4-Amino-N'-(2-hydroxy-5-methoxy-benzylidene)benzohydrazide monohydrate
    Kargar, Hadi
    Kia, Reza
    Tahir, Muhammad Nawaz
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02321 - +
  • [26] (E)-5-[(2-Hydroxy-5-methoxybenzylidene)amino]-1,3,4-thiadiazole-2(3H)-thione
    Kargar, Hadi
    Kia, Reza
    Tahir, Muhammad Nawaz
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3311 - U1226
  • [27] 1-(2-Hydroxy-5-methoxyphenyl)-3methylbut-2-en-1-one(1)
    Alexander, Catherine Thomas
    Vargas, David
    Fronczek, Frank R.
    Watkins, Steven F.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O3126 - +
  • [28] (4-Fluorophenyl)(2-hydroxy-5-methylphenyl) methanone
    Dileep, C. S.
    Ranganatha, V. Lakshmi
    Lokanath, N. K.
    Khanum, S. A.
    Sridhar, M. A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O286 - +
  • [29] tert-Butyl N-((1S)-2-hydroxy-1-{N′-[(E)-2-hydroxy-4-methoxybenzylidene]-hydrazinecarbonyl}ethyl) carbamate
    Wardell, James L.
    de Souza, Marcus V. N.
    Pinheiro, Alessandra C.
    Tiekink, Edward R. T.
    Wardell, Solange M. S. V.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1888 - U1667
  • [30] (E)-5-[(2-Hydroxy-3-methoxybenzylidene)amino]-1,3,4-thiadiazole-2(3H)-thione
    Kargar, Hadi
    Kia, Reza
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3518 - U1420
12345