THE WITTIG REACTION OF STABLE YLIDE WITH ALDEHYDE UNDER MICROWAVE IRRADIATION - SYNTHESIS OF ETHYL CINNAMATES

被引：74

作者：

XU, CD ^{[1
]}

CHEN, GY ^{[1
]}

FU, C ^{[1
]}

HUANG, XA ^{[1
]}

机构：

[1] HANGZHOU UNIV,DEPT CHEM,ZHEJIANG 310028,PEOPLES R CHINA

来源：

SYNTHETIC COMMUNICATIONS | 1995年 / 25卷 / 15期

关键词：

D O I：

10.1080/00397919508011778

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The Wittig reaction of stable ylide, triphenylcarbethoxymethylene phosphorane, with aldehydes was performed within 5-6 minutes under microwave irradiation. Remarkable rate enhancements and dramatic reductions of reaction times have been observed. Thus, the Wittig reaction of stable ylide with aldehyde is optimized.

引用

页码：2229 / 2233

页数：5

共 13 条

[1] WET ASHING OF SOME BIOLOGICAL SAMPLES IN A MICROWAVE OVEN [J].

ABUSAMRA, A ;

MORRIS, JS ;

KOIRTYOHANN, SR .

ANALYTICAL CHEMISTRY, 1975, 47 (08) :1475-1477

[2]

[Anonymous], 1989, MERCK INDEX

[3] FUME SCRUBBER FOR A MODIFIED MICROWAVE OVEN FOR WET ASHING BIOLOGICAL SAMPLES [J].

COOLEY, TN ;

MARTIN, DF ;

QUINCEL, RH .

JOURNAL OF ENVIRONMENTAL SCIENCE AND HEALTH PART A-ENVIRONMENTAL SCIENCE AND ENGINEERING & TOXIC AND HAZARDOUS SUBSTANCE CONTROL, 1977, 12 (1-2) :15-19

[4] MICROWAVE DISSOLUTION OF GEOLOGIC MATERIAL - APPLICATION TO ISOTOPE-DILUTION ANALYSIS [J].