RESEARCH ON NITROGEN AND SULFUR HETEROCYCLIC-COMPOUNDS - SYNTHESIS OF 10H-PYRROLO[1,2-A]THIENO[3,4-E][1,4]-DIAZEPIN-5(4H)-ONE AND SOME DERIVATIVES

被引:2
作者
DAICH, A
MOREL, J
DECROIX, B
机构
[1] Laboratoire de Chimie, UER des Sciences et des Techniques, Université du Havre, Le Havre, 76600
关键词
D O I
10.1002/jhet.5570310214
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
The synthesis of 10H-pyrrolo[1,2-a]thieno[3,4-e][1,4]diazepin-5(4H)-one (16) and some derivatives are described from methyl 3-bromomethylthiophene-4-carboxylate (5). The key step of these sequences is the intramolecular cyclization of the carbonylazides 12 and 13.
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页码:341 / 344
页数:4
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