Bis(4-benzoyl-3-methyl-1-phenyl-4,5-dihydro-1H-pyrazol-5-olato-kappa O-2,O ')-(methanol-kappa O)dioxidouranium(VI) methanol monosolvate

被引：0
|
作者：
Dehbi, Ouarda [1 ]
Keraghel, Saida [1 ]
Bouacida, Sofiane [2 ]
Benghanem, Fatiha [1 ]
Ourari, Ali [1 ]
机构：
[1] Univ Farhat Abbas, Fac Sci Ingn, LEIMCR, Setif 19000, Algeria
[2] Univ Mentouri Constantine, CHEMS, Unite Rech Chim Environnement & Mole Struct, Setif 25000, Algeria
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词：
D O I：
10.1107/S1600536812011075
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, [U(C17H13N2O2)(2)O-2(CH3OH)]center dot CH3OH, the U-VI ion is coordinated by seven O atoms in a distorted pentagonal-bipyramidal geometry with two 3-methyl-1-phenyl-4-benzoyl-4,5-dihydro-1H-pyrazol-5-olate groups with two O atoms in a bidentate chelating coordination mode and by three O atoms, one of which is from a methanol ligand. The crystal packing can be described by alternating layers of complex molecules along the a axis. The structure is stabilized by O-H center dot center dot center dot N and O-H center dot center dot center dot O hydrogen bonding and van der Waals interactions.
引用
收藏
页码：M457 / +
页数：12
相关论文
共 50 条
  • [31] Crystal structure of chlorido{1-(2,3-dimethyl-5-oxido-1-phenyl-1H-pyrazol-2-ium-4-yl-kappa O)-2-[3-methyl-5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-4-ylidene-kappa O]hydrazin-1-ido-kappa N-1}copper(II) from laboratory X-ray powder data
    Kovalchukova, Olga
    Van Nguen
    Strashnova, Svetlana
    Kuznetsov, Dmitry
    Berikashvili, Teimuraz
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : 124 - +
  • [32] Bis(N,N-dimethylformamide-κO)bis[1-phenyl-3-methyl-4-benzoyl-1H-pyrazol-5(4H)-onato-κ2O,O′]nickel(II)
    Shen, XP
    Yuan, AH
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2004, 60 : M1228 - M1230
  • [33] Hexa-mu-acetato-1:2 kappa O-4,O';1:2 kappa O-2:O;2:3 kappa O-4,O';2:3 kappa O-2:O-bis(4,4'-dimethyl-2,2'-bipyridine)-1 kappa N-2,N';3 kappa N-2,N'-2-calcium-1,3-dizinc
    Pramanik, Avijit
    Fronczek, Frank R.
    Venkatraman, Ramaiyer
    Hossain, Md. Alamgir
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : M643 - +
  • [34] Polymeric (aqua-1 kappa O)bis[(R,R)-tartrato-1 kappa(2) O-1,O-2:2 kappa(2) O-3,O-4]dimanganese(II) trihydrate
    RuizPerez, C
    HernandezMolina, M
    GonzalezSilgo, C
    Lopez, T
    Yanes, C
    Solans, X
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1996, 52 : 2473 - 2475
  • [35] Poly[tetraaquabis(mu(3)-oxalato-kappa O-5,O-2:O-1':O-1',O-2'('))(mu(2)-oxalato-kappa(4) O-1,O-2:O-1',O-2') dipraseodymium(III)]
    Hao, Cheng-Jun
    Xie, Hui
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : M444 - +
  • [36] Bis(mu-3-nitrophthalato-kappa O-2(1):O-2)bis-[(thiourea-kappa S) zinc] dihydrate
    Gao, Hui-Peng
    Guo, Ming-Lin
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : M264 - U491
  • [37] BIS(ETHANOL)-1-KAPPA-O,4-KAPPA-O-HEXAKIS(MU-PROPIONATO)-1-KAPPA-O-2-KAPPA-O'2-KAPPAO-4-3-KAPPA-O-4'-3-KAPPA-O-4-KAPPA-O'-TETRAKIS(TRIPHENYLPHOSPHINE)-1-KAPPA-P-2,4-KAPPA-P-2-TETRACOPPER(I,II),[CU-4(C3H5O2)6(C2H6O2)(C18H15P)(4)]
    DUNAJJURCO, M
    KOMAN, M
    VALIGURA, D
    ONDREJOVIC, G
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1995, 51 : 1082 - 1084
  • [38] Tetraaquabis(N,N-dimethylformamide-kappa O)zinc(II) bis[(2-{3-[2-(carboxylatomethoxy-kappa O-2,O ')phenyl]pyrazol-1-yl-kappa N-2}acetato-kappa O)chloridozincate(II)]
    Yang, Jie
    Shen, Lei
    Ji, Cheng
    Shen, Xiao-Feng
    Yang, Gao-Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : M817 - +
  • [39] Crystal structure of bis(μ2-1-(4-chlorophenyl)-3-phenyl-4-thenoyl-1H-pyrazol-5-olato-κ3O,O′:O′)-bis-(1-(4-chlorophenyl)-3-phenyl-4-thenoyl-1H-pyrazol-5-olato- κ2O,O)-bis(ethyl acetate-κO) dicadmium(II), C88H64Cl4N8O12S4Cd2
    Ding, Yong-Jie
    Zhao, Chun-Xiang
    Hu, Si-Shi
    Wang, Peng-Hui
    Ye, Chen-Cheng
    Jia, Hua-Li
    Chen, Guang-Ying
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2019, 234 (03): : 477 - 479
  • [40] Di-mu-nicotinamide-kappa N-2(1):O; kappa(2) O:N-1-bis[aquabis(3-chlorobenzoato-kappa O-2, O')cadmium]
    Bozkurt, Nihat
    Dilek, Nefise
    Delibas, Nagihan Caylak
    Necefoglu, Hacali
    Hokelek, Tuncer
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : M389 - +
12345