DETERMINATION OF MILLIGRAM AMOUNTS OF THIOUREA, ALLYLTHIOUREA AND PHENYLTHIOUREA USING N-CHLOROSACCHARIN IN ACETIC-ACID MEDIUM

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作者
CHAUHAN, RPS [1 ]
AHMED, I [1 ]
KUMAR, A [1 ]
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[1] GAYA COLL,DEPT CHEM,POSTGRAD CTR,GAYA 823001,BIHAR,INDIA
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A quick and convenient method has been developed for the micro determination of thiourea and some of its derivatives, milligram amount of the sample is allowed to react with excess of N-chlorosaccharin at room temperature for 10 min. After the reaction is over, the unconsumed reagent is back titrated iodometrically.
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页码:667 / 668
页数:2
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