Crystal structure of supramolecular complexes formed by 18-crown-6 and cis-anti-cis-dicyclohexano-18-crown-6 (host) with 3,4-diaminofurazane (guest)

被引：8
|
作者：
Luboradzki, R
Lipkowski, J
Simonov, YA
Fonari, MS
Ganin, EV
Yavolovskii, AA
机构：
[1] MOLDAVIAN ACAD SCI,INST APPL PHYS,KISHINEV 277028,MOLDOVA
[2] ODESSA II MECHNIKOV STATE UNIV,INST ENVIRONM & HUMAN PROTECT,ODESSA 270100,UKRAINE
来源：
JOURNAL OF INCLUSION PHENOMENA AND MOLECULAR RECOGNITION IN CHEMISTRY | 1995年 / 23卷 / 03期
关键词：
18-crown-6; diaminofurazane; crystal structure; host-guest complexes;
D O I：
10.1007/BF00709576
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An X-ray-diffraction study is reported for two molecular complexes containing 3,4-diamino-1,2,5-oxadiazole as guest (G) with 18-crown-6 (18-C-6) and cis-anti-cis-dicyclohexano-18-crown-6 (DCH-6B) as host. Both complexes are of the polymeric-chain structure with the guest molecule bridging two crown neighbours. Complex I: [18-C-6 * G * H2O], 1:1:1, monoclinic, P2(1)/n, a = 8.171(1), b = 15.042(2), c = 16.209(6) Angstrom, beta = 101.15(2)degrees, final R-factor 0.068. Complex II: [DCH-6B * G], 1:1, monoclinic C2/c, a = 21.212(4), b = 9.380(2), c = 13.049(3) A, beta = 108.61(3)degrees, final R 0.047.
引用
收藏
页码：181 / 193
页数：13
相关论文
共 50 条
  • [41] SYNTHESIS AND CRYSTAL-STRUCTURE OF [(CLAL-MU-OH)2ALCL).18-CROWN-6][ALCL4]2.8 3C6H5NO2, A COMPLEX FEATURING A BINUCLEAR ALUMINUM-CONTAINING CATION THREADED THROUGH 18-CROWN-6
    ATWOOD, JL
    BOTT, SG
    MAY, MT
    JOURNAL OF COORDINATION CHEMISTRY, 1991, 23 (1-4) : 313 - 320
  • [42] Studies on polyhalides, XXXIX -: Structure refinement of [(H3O)(18-crown-6)]I7
    Abd El Khalik, S
    El Essawi, M
    Dombrowski, I
    Tebbe, KF
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1999, 54 (01): : 136 - 139
  • [43] Crystal structure of diaqua[5,10,15,20-tetrakis(4-methoxyphenyl)porphyrinato-kappa N-4]iron(III) diaqua(18-crown-6)-potassium bis(trifluoromethanesulfonate)-18-crown-6 (1/2)
    Hassen, Leila Ben Haj
    Denden, Zouhour
    Roussclin, Yoann
    Nasri, Habib
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : M215 - U154
  • [44] Synthesis and Crystal Structures of New 18-Crown-6 Complexes With M2[Sn(i-mnt)3](M = K, Na)
    Kong, Lingqian
    Xu, Jianzhong
    Li, Shengli
    Li, Dacheng
    Dou, Jianmin
    SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2016, 46 (04) : 617 - 621
  • [45] On iodido bismuthates, bismuth complexes and polyiodides with bismuth in the system Bil3/18-crown-6/I2
    Notter, Silke
    Donsbach, Carsten
    Feldmann, Claus
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 2021, 76 (10-12): : 765 - 774
  • [46] Crystal Structure of the Bis(Picrato-O,O")Tetraaquacalcium Complex with 18-Crown-6, [Ca(Pic)2(H2O)4] · 18C6
    A. N. Chekhlov
    Russian Journal of Coordination Chemistry, 2001, 27 : 762 - 766
  • [47] Molecular structure of bis[(1,3)2-oxaadamantano]-18-crown-6 and its potassium picrato complex
    Mlinaric-Majerski, K
    Visnjevac, A
    Kragol, G
    Kojic-Prodic, B
    JOURNAL OF MOLECULAR STRUCTURE, 2000, 554 (2-3) : 279 - 287
  • [48] CRYSTAL-STRUCTURE OF THE 1-4 COMPLEX BETWEEN 18-CROWN-6 AND A POLYFUNCTIONAL GUEST - 2-HYDROXYMETHYL-4-(1,1,3,3-TETRAMETHYLBUTYL)PHENOL
    PERRIN, M
    MAHDAR, E
    LECOCQ, S
    BAVOUX, C
    JOURNAL OF INCLUSION PHENOMENA AND MOLECULAR RECOGNITION IN CHEMISTRY, 1990, 9 (02): : 153 - 160
  • [49] Synthesis and Structural Phase Transitions of Copper(II) and Iron(III) Complexes Containing [(C8H12NO)(18-crown-6)]+ Supramolecular Cations
    Jin, Yu
    Yu, Chun-Hua
    Wang, Yu-Feng
    Li, Si-Chao
    Zhang, Wen
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2014, 640 (07): : 1499 - 1505
  • [50] Synthesis and crystal structure of the monomeric in-cavity complex [SmI3(dibenzo-18-crown-6)]
    Runschke, C
    Meyer, G
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1997, 623 (06): : 981 - 984
12345