THE CRYSTAL-STRUCTURE OF 2,5-DICHLORO-3-METHOXY-6-(1'-TRIPHENYLPHOSPHONIO-CYCLOPENTADIEN-3-YL)-P-BENZOQUINONE

被引：2

作者：

HALL, CD

SHERIDAN, A

SHEK, L

PARKINS, AW

NYBURG, SC

机构：

[1] Department of Chemistry, King's College, Strand

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 1992年 / 69卷 / 1-2期

关键词：

TRIPHENYLPHOSPHINO CYCLOPENTADIENIDE; QUINONE DERIVATIVE; X-RAY CRYSTALLOGRAPHY; CHLORANIL;

D O I：

10.1080/10426509208036866

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A single crystal X-ray diffraction study confirms that the reaction of triphenylphosphonio cyclopenta-dienide 1 with 3-methoxy-2, 5, 6-trichloro-p-benzoquinone 4 gives a product 5 with the cyclopentadiene ring substituted in position 3 and the chlorine atoms of the quinone ring replaced at positions 3 and 6. This data confirms the prediction of earlier multinuclear 2D nmr data on the reaction of 1 with chloranil. © 1992, Taylor & Francis Group, LLC. All rights reserved.

引用

页码：167 / 172

页数：6

共 44 条

[1] Crystal structure of 4,7-dichloro-1,2,3,5,6,8-hexakis-(4-methoxy-phenylsulfanyl)-acenaphthylene
Deng, Shun-Liu
Li, Sa
Huang, Rong-Bin
Zheng, Lan-Sun
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2008, 38 (09) : 679 - 683
[2] Crystal Structure of 4,7-Dichloro-1,2,3,5,6,8-hexakis-(4-methoxy-phenylsulfanyl)-acenaphthylene
Shun-Liu Deng
Sa Li
Rong-Bin Huang
Lan-Sun Zheng
Journal of Chemical Crystallography, 2008, 38 : 679 - 683
[3] Crystal structure of 4-(1-methyl-1-mesitylcyclobutane-3-yl)-2-aminothiazole
Aksoy, I
Yilmaz, I
Sari, U
Güven, K
Çukurovali, A
CRYSTAL RESEARCH AND TECHNOLOGY, 2006, 41 (03) : 293 - 298
[4] Synthesis and crystal structure of 2,5-bis(morpholino)-3,4-bis(p-chlorophenyl)thiophene
Zeng, RS
Zou, JP
Wang, XS
Mo, XJ
Lu, ZE
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2003, 22 (03) : 279 - 282
[5] Synthesis and Crystal Structure of 2,5-Bis(morpholino)-3,4-bis(p-chlorophenyl)thiophene
ZENG Run-Shenga ZOU Jian-Pinga② WANG Xiang-Shanb MO Xue-Juna LU Zhong-Ea a (Department of Chemistry
结构化学, 2003, (03) : 279 - 282
[6] Stoichiometric, Thermodynamic and Computational DFT Analysis of Charge Transfer Complex of 1-Benzoylpiperazine with 2, 3-Dichloro-5, 6-Dicyano-1, 4-benzoquinone
Abbu, Venugopal
Nampally, Venkatesh
Baindla, Naveen
Tigulla, Parthasarathy
JOURNAL OF SOLUTION CHEMISTRY, 2019, 48 (01) : 61 - 81
[7] Synthesis, Crystal Structure, and DFT Study of 3-(2-Naphthol-1-yl) naphtho[2,1-b]furan
Niroomand, Sahar
Behmadi, Hossein
Pordel, Mehdi
Allameh, Sadegh
INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2023, 33 (04) : 397 - +
[8] Crystal and electronic structure of heteromolecular complexes of 3,6-bis(3,5-dymethylpyrazole-1-yl)-1,2,4,5-tetrazine with azoles
P. A. Slepukhin
E. S. Salmina
V. A. Potemkin
M. A. Grishina
Journal of Structural Chemistry, 2013, 54 : 1091 - 1100
[9] Crystal and electronic structure of heteromolecular complexes of 3,6-bis(3,5-dymethylpyrazole-1-yl)-1,2,4,5-tetrazine with azoles
Slepukhin, P. A.
Salmina, E. S.
Potemkin, V. A.
Grishina, M. A.
JOURNAL OF STRUCTURAL CHEMISTRY, 2013, 54 (06) : 1091 - 1100
[10] THE X-RAY CRYSTAL-STRUCTURE AND PACKING MODE OF (+/-)-2-THIONO-2-MERCAPTO-A,A'-DINAPHTHO(D,F)(1,3,2)DIOXOPHOSPHEPIN - A CLATHRATE STRUCTURE
GONG, BQ
CHEN, WY
HU, BF
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1991, 57 (1-2) : 87 - 94

← 1 2 3 4 5 →