THE ROLE OF THE INITIAL REAGENTS IN THE LOW-O2 PRESSURE SYNTHESIS OF YBA2CU4O8

被引:2
作者
BONOLDI, L
SPARPAGLIONE, M
ZINI, L
机构
[1] Enichem, Novara, 28100
关键词
D O I
10.1007/BF01162486
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A comparative analysis of the effect of the starting reagents in the synthesis of YBa2Cu4O8 (124) is presented. Eight different combinations of salts and oxides of the elements in the initial composition were studied. It is shown that all the syntheses starting with;copper nitrate give 124 in approximately 80 h of treatment with only small amounts of CuO and Y2BaCuO5 impurities. Longer times are needed if CuO is used as a starting reagent.
引用
收藏
页码:324 / 327
页数:4
相关论文
共 14 条
[1]   SYNTHESIS OF 80-K SUPERCONDUCTING YBA2CU4O8 VIA A NOVEL ROUTE [J].
BALACHANDRAN, U ;
BIZNEK, ME ;
TOMLINS, GW ;
VEAL, BW ;
POEPPEL, RB .
PHYSICA C, 1990, 165 (3-4) :335-339
[2]   SPECIFIC-HEAT, MAGNETIZATION AND RESISTIVITY MEASUREMENTS ON HOBA2CU4O8 [J].
BERNASCONI, A ;
SCHILLING, A ;
GUO, JD ;
OTT, HR .
PHYSICA C, 1990, 166 (5-6) :393-398
[3]   SYNTHESIS OF BULK SUPERCONDUCTING YBA2CU4O8 AT ONE ATMOSPHERE OXYGEN-PRESSURE [J].
CAVA, RJ ;
KRAJEWSKI, JJ ;
PECK, WF ;
BATLOGG, B ;
RUPP, LW ;
FLEMING, RM ;
JAMES, ACWP ;
MARSH, P .
NATURE, 1989, 338 (6213) :328-330
[4]   ON THE PREPARATION OF Y1BA2CU4O8 [J].
HORN, J ;
BORNER, H ;
SEMMELHACK, HC ;
LIPPOLD, B ;
HERRMANN, J ;
WURLITZER, M ;
KROTZSCH, M ;
BOEHNKE, U ;
SCHLENKRICH, F ;
FRENZEL, C .
SOLID STATE COMMUNICATIONS, 1991, 79 (06) :483-486
[5]   FORMATION MECHANISM STUDY OF YBA2CU4O8+ALPHA,DYBA2CU4O8+ALPHA ACCELERATED BY NITRIC-ACID [J].
HURNG, WM ;
WU, SF ;
SHEI, CY ;
HUANG, YT ;
LEE, WH .
APPLIED PHYSICS LETTERS, 1990, 57 (19) :2025-2027
[6]   SYNTHESIS AND PROPERTIES OF THE YBA2CU4O8 SUPERCONDUCTOR [J].
JIN, S ;
OBRYAN, HM ;
GALLAGHER, PK ;
TIEFEL, TH ;
CAVA, RJ ;
FASTNACHT, RA ;
KAMMLOTT, GW .
PHYSICA C, 1990, 165 (5-6) :415-418
[7]   EQUILIBRIUM PRESSURES OF OXYGEN ABOVE YBA2CU3O7+/-X UP TO 2,000 BAR [J].
KARPINSKI, J ;
KALDIS, E .
NATURE, 1988, 331 (6153) :242-245
[8]   THE HIGH-TC SUPERCONDUCTING PHASES OF THE Y2BA4CU6+NO14+N FAMILY [J].
KARPINSKI, J ;
RUSIECKI, S ;
KALDIS, E ;
JILEK, E .
JOURNAL OF THE LESS-COMMON METALS, 1990, 164 :3-19
[9]   SYNTHESIS OF YBA2CU4O8 AT ONE ATMOSPHERE OXYGEN-PRESSURE BY THE MODIFIED CITRATE GEL PROCESS [J].
LIU, RS ;
JANES, R ;
BENNETT, MJ ;
EDWARDS, PP .
APPLIED PHYSICS LETTERS, 1990, 57 (09) :920-921
[10]   SYNTHESIS OF A BULK YBA2CU4O8 SUPERCONDUCTOR BY ADDITION OF AG2O AT AN ORDINARY PRESSURE OF OXYGEN [J].
OHARA, S ;
MATSUDA, M ;
WATANABE, Y ;
TAKATA, M .
APPLIED PHYSICS LETTERS, 1991, 59 (05) :603-605