Crystal structure of 1,4,5,6,7,8,9,10,11,1 2,13-undecahydrocyclododeca[c]pyrazol-3-ol

被引：0

作者：

Raymond, Casey C. ^{[1
]}

Knopp, Michael A. ^{[2
]}

机构：

[1] SUNY Coll Oswego, Dept Chem, 296 Shineman Ctr, Oswego, NY 13126 USA

[2] Univ Maine, Environm Sci & Sustainabil Dept, Presque Isle, ME 04769 USA

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2015年 / 71卷

关键词：

crystal structure; pyrazolol; tautomer; pyrazolone; macrocycle; O-H center dot center dot center dot N hydrogen bond; N-H center dot center dot center dot pi interaction;

D O I：

10.1107/S2056989015016746

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C13H22N2O, crystallized as a pyrazolol tautomer. The 12-membered macrocycle has a distorted chair conformation. In the crystal, molecules are linked via pairs of O-H center dot center dot center dot N hydrogen bonds, forming inversion dimers. The dimers are linked via N-H center dot center dot center dot pi and C-H center dot center dot center dot pi interactions, forming slabs parallel to the be plane.

引用

页码：O752 / U387

页数：8

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