BENZO[C]CINNOLINES .3. HALOGENATION STUDIES - NMR SPECTROSCOPIC STUDY OF BENZO[C]CINNOLINE AND ITS MONOBROMO-DERIVATIVES

被引：13

作者：

BARTON, JW

LAPHAM, DJ

机构：

[1] School of Chemistry, The University

来源：

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1 | 1979年 / 06期

关键词：

D O I：

10.1039/p19790001503

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Electrophilic bromination and chlorination of benzo[c]cinnoline in sulphuric acid give mixtures of 1-and 4-halogenobenzo[c]cinnolines, then 1,4-dihalogenobenzo[c]cinnolines. The 1H n.m.r. spectra of the monobromobenzo[c]-cinnolines have been analysed and previous assignments made for the parent benzo[c]cinnoline are corrected.

引用

收藏

页码：1503 / 1505

页数：3

相关论文

共 15 条

[1] SYNTHESIS OF NITRO AND AMINO DERIVATIVES OF BENZO[C]CINNOLINE [J].

ARCOS, JC ;

ARCOS, M ;

MILLER, JA .

JOURNAL OF ORGANIC CHEMISTRY, 1956, 21 (06) :651-654

[2] PHOTOCHEMICAL REACTIONS OF AZO COMPOUNDS .3. PHOTOCHEMICAL CYCLODEHYDROGENATIONS OF SUBSTITUTED AZOBENZENES [J].

BADGER, GM ;

LEWIS, GE ;

DREWER, RJ .

AUSTRALIAN JOURNAL OF CHEMISTRY, 1964, 17 (09) :1036-&

[3] BENZO(C)CINNOLINES .PART 2. SYNTHESIS REACTIONS OF SOME BENZO)C)CINNOLINE OXIDES [J].

BARTON, JW ;

THOMAS, JR .

JOURNAL OF THE CHEMICAL SOCIETY, 1964, (APR) :1265-&

[4] BENZO[C]CINNOLINES - NIRATION OF BENZO[C]CINNOLINE AND ITS N-OXIDE [J].

BARTON, JW ;

COCKETT, MA .

JOURNAL OF THE CHEMICAL SOCIETY, 1962, (JUN) :2454-&

[5] SYNTHESIS OF 4-HALOPHENANTHRENES AND 4,5-PHENANTHRYLENEIODONIUM SALTS [J].

BERINGER, FM ;

CHANG, LL ;

FENSTER, AN ;

ROSSI, RR .

TETRAHEDRON, 1969, 25 (18) :4339-&

[6] THE PROTON MAGNETIC RESONANCE SPECTRA OF CONJUGATED AROMATIC HYDROCARBONS [J].

BERNSTEIN, HJ ;

SCHNEIDER, WG ;

POPLE, JA .

PROCEEDINGS OF THE ROYAL SOCIETY OF LONDON SERIES A-MATHEMATICAL AND PHYSICAL SCIENCES, 1956, 236 (1207) :515-528

[7] POLYCYCLIC CINNOLINE DERIVATIVES .9. BROMINATION OF BENZO[C]CINNOLINE AND PREPARATION AND ULTRAVIOLET ABSORPTION SPECTRA OF REFERENCE COMPOUNDS [J].

CORBETT, JF ;

HOLT, PF .

JOURNAL OF THE CHEMICAL SOCIETY, 1961, (NOV) :5029-&

[8]

CORBETT JF, 1962, J CHEM SOC, P949

[9] POLYCYCLIC CINNOLINE DERIVATIVES .17. ULTRAVIOLET ABSORPTION OF BROMOBENZO[C]CINNOLINES AND THEIR OXIDES [J].

HOLT, PF ;

OAKLAND, R .

JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC, 1966, (15) :1306-&

[10] SYNTHESIS, REACTIONS AND FLUXIONAL BEHAVIOR OF SOME BENZO[C]CINNOLINE AND PHENANTHRIDINE PENTACARBONYL COMPLEXES OF CHROMIUM, MOLYBDENUM AND TUNGSTEN [J].

KOOTI, M ;

NIXON, JF .

JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1976, 105 (02) :217-230