CHEMICAL SYNTHESIS OF P-NITROPHENYL BETA-SOPHOROSIDE AND P-NITROPHENYL BETA-LAMINARABIOSIDE

被引：7
作者：
IYER, RN
GOLDSTEIN, IJ
机构：
[1] Department of Biological Chemistry, The University of Michigan, Ann Arbor
来源：
CARBOHYDRATE RESEARCH | 1969年 / 11卷 / 02期
关键词：
D O I：
10.1016/S0008-6215(00)80080-4
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
Condensation of tetra-O-acetyl-α-d-glucopyranosyl bromide with p-nitrophenyl 4,6-O-benzylidene-β-d-glucopyranoside followed by appropriate deblocking reactions gives rise to an approximately equimolar mixture of p-nitrophenyl β-sophoroside and p-nitrophenyl β-laminarabioside. The two glycosides are readily separated and isolated in pure form by cellulose-column chromatography. © 1969.
引用
收藏
页码：241 / +
页数：1
相关论文
共 50 条
[41]   Micelle effects of functionalized surfactants, 1-cetyl-3-(2-hydroxyiminopropyl)imidazolium halides, in reactions with p-nitrophenyl p-toluenesulfonate, diethyl p-nitrophenyl phosphate, and ethyl p-nitrophenyl ethylphosphonate [J].
Simanenko, YS ;
Popov, AF ;
Karpichev, EA ;
Prokop'eva, TM ;
Savelova, VA ;
Bunton, CA .
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2002, 38 (09) :1314-1325
[42]   INHIBITION OF CHYMOTRYPTIC HYDROLYSIS OF P-NITROPHENYL ACETATE [J].
FOSTER, RJ .
FEDERATION PROCEEDINGS, 1958, 17 (01) :222-222
[43]   ACETYLATION OF CREATINE PHOSPHOKINASE WITH P-NITROPHENYL ACETATE [J].
CLARK, JR ;
CUNNINGH.L .
BIOCHEMISTRY, 1965, 4 (12) :2637-&
[44]   Micelle Effects of Functionalized Surfactants, 1-Cetyl-3-(2-hydroxyiminopropyl)imidazolium Halides, in Reactions with p-Nitrophenyl p-Toluenesulfonate, Diethyl p-Nitrophenyl Phosphate, and Ethyl p-Nitrophenyl Ethylphosphonate [J].
Yu. S. Simanenko ;
A. F. Popov ;
E. A. Karpichev ;
T. M. Prokop'eva ;
V. A. Savelova ;
C. A. Bunton .
Russian Journal of Organic Chemistry, 2002, 38 :1314-1325
[45]   Mechanism of the hydrolysis of α-(p-nitrophenyl)cinnamonitrile derivatives [J].
Pyun, S.-Y. ;
Kim, T.-R. ;
Kwon, H.-S. ;
Lee, S.-H. .
KINETICS AND CATALYSIS, 2007, 48 (05) :626-631
[46]   A mechanistic study for aminolysis of p-nitrophenyl phenylacetate [J].
Um, IH ;
Yeom, ES ;
Kwon, HJ ;
Kwon, DS .
BULLETIN OF THE KOREAN CHEMICAL SOCIETY, 1997, 18 (08) :865-868
[47]   Mechanism of the hydrolysis of α-(p-nitrophenyl)cinnamonitrile derivatives [J].
S. -Y. Pyun ;
T. -R. Kim ;
H. -S. Kwon ;
S. -H. Lee .
Kinetics and Catalysis, 2007, 48 :626-631
[48]   IDENTIFICATION OF P-NITROPHENYL GLUCOSIDE AS A URINARY METABOLITE [J].
GESSNER, T ;
HAMADA, N .
JOURNAL OF PHARMACEUTICAL SCIENCES, 1970, 59 (10) :1528-&
[49]   p-nitrophenyl α-D-mannopyranoside hemihydrate [J].
CSIC, Madrid, Spain .
Acta Crystallogr Sect C Cryst Struct Commun, 6 (1586-1588)
[50]   BULK FERROMAGNETISM OF P-NITROPHENYL NITRONYL NITROXIDE [J].
KINOSHITA, M .
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1995, 209 :284-PMSE
12345