THE DESIGN SYNTHESIS AND CRYSTALLOGRAPHIC CHARACTERIZATION OF A NOVEL HETEROTRIMETALLIC LINEAR COMPLEX OF [ET4N][(PH3P)2(CUS2MOS2FE)CL2]

被引:8
作者
SHENG, TL [1 ]
DU, SW [1 ]
WU, XT [1 ]
机构
[1] CHINESE ACAD SCI,FUJIAN INST RES STRUCT MATTER,STATE KEY LAB STRUCT CHEM,FUZHOU 350002,PEOPLES R CHINA
基金
中国国家自然科学基金;
关键词
D O I
10.1016/S0277-5387(00)87060-6
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The complex [Et4N][(Ph3P)2{CuS2MoS2Fe}Cl2] has been obtained by reaction of [Et4N]2[S2MoS2FeCl2] with Cu(PPh3)3Cl in MeCN/CH2Cl2. In this new complex, the bond lengths of the Mo-Fe bond and the Mo-Cu bond are 2.769(2) and 2.786(2) angstrom, respectively.
引用
收藏
页码:111 / 115
页数:5
相关论文
共 42 条
[1]   PREPARATION, CRYSTAL-STRUCTURE, AND SPECTROSCOPIC STUDIES OF [NPRN4]2[(PHS)CUS2MOS2] AND [NPRN4]2[(PHS)CUS2MOS2CU(SPH)], CONTAINING BENZENETHIOLATOCOPPER(I) TETRATHIOMOLYBDATE(VI) COMPLEX ANIONS [J].
ACOTT, SR ;
GARNER, CD ;
NICHOLSON, JR ;
CLEGG, W .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1983, (04) :713-719
[2]  
BEURSKENS PT, 1984, 19841 CRYST LAB TECH
[3]   COPPER-MOLYBDENUM ANTAGONISM IN RUMINANTS .1. FORMATION OF THIOMOLYBDATES IN ANIMAL RUMEN [J].
CLARKE, NJ ;
LAURIE, SH .
JOURNAL OF INORGANIC BIOCHEMISTRY, 1980, 12 (01) :37-43
[5]  
COUCOUVANIS D, 1980, J AM CHEM SOC, V102, P7132
[6]  
Cromer D.T, 1974, INT TABLES XRAY CRYS, VIV
[7]  
DU SW, 1992, J CHEM SOC DALTON, P339
[8]  
DU SW, 1992, POLYHEDRON, V11, P109
[9]   SYNTHESIS AND CHARACTERIZATION OF COMPLEXES OF THIOMOLYBDATES AND THIOTUNGSTATES WITH COPPER(I) AND SILVER(I) CYANIDES, INCLUDING MO-95 AND W-183 NMR PROPERTIES AND THE CRYSTAL AND MOLECULAR-STRUCTURES OF (N-PR4N)2[(CN)CUS2MOS2], (N-PR4N)2[(CN)AGS2WS2], AND (PH4AS)2[(CN)CUS2MOS2CU(CN)].H2O [J].
GHELLER, SF ;
HAMBLEY, TW ;
RODGERS, JR ;
BROWNLEE, RTC ;
OCONNOR, MJ ;
SNOW, MR ;
WEDD, AG .
INORGANIC CHEMISTRY, 1984, 23 (16) :2519-2528
[10]  
GILMORE CJ, 1983, MITHRIL COMPUTER PRO