Crystal Structure of 1,2-Bis[N,N '-6-(3-pyridylmethylamido)pyridyl-2-carboxy-amido]ethane

被引：1
|
作者：
Kadir, Maisara Abdul [1 ]
Yusof, M. Sukeri M. [1 ]
Sumby, C. J. [2 ]
机构：
[1] Univ Malaysia Terengganu, Sch Fundamental Sci, Kuala Nerus 21030, Terengganu, Malaysia
[2] Univ Adelaide, Sch Phys Sci, Ctr Adv Nanomat, Adelaide, SA 5005, Australia
来源：
X-RAY STRUCTURE ANALYSIS ONLINE | 2018年 / 34卷
关键词：
D O I：
10.2116/xraystruct.34.31
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
Compound 1, namely 1,2-bis[N,N'-6-(3-pyridylmethylamido)pyridyl-2-carboxyamido]ethane, crystallizes in the space group C2/c, with cell parameters a = 13.669(6)angstrom, b = 17.763(7)angstrom, c = 11.013(4)angstrom, beta = 108.857(16), Z = 4, and V = 2530.5(17)angstrom(3). The asymmetric unit comprises half of the title compound with the compound adopting a U-shaped conformation stabilized by intramolecular hydrogen bonding. Crystal packing is governed by N-H center dot center dot center dot N and C-H center dot center dot center dot O hydrogen bonds. The structure has been solved and refined to reach R and wR indices for all data of 0.0514 and 0.1366, respectively.
引用
收藏
页码：31 / 32
页数：2
相关论文
共 50 条
  • [31] THE CRYSTAL AND MOLECULAR-STRUCTURE OF 1,2-BIS(DIPHENYLPHOSPHINO)ETHANE-BIS(TRIMETHYLGALLIUM)
    BOARDMAN, A
    SMALL, RWH
    WORRALL, IJ
    INORGANICA CHIMICA ACTA, 1986, 119 (01) : L13 - L14
  • [32] X-ray crystal structure of 1,2-bis[bis(2-methylthiophenyl)phosphino]ethane
    Laitinen, RH
    Losonczi, J
    Pursiainen, J
    Ahlgren, M
    ACTA CHEMICA SCANDINAVICA, 1997, 51 (6-7): : 804 - 806
  • [33] Crystal　Structure　of　μ－［meso－1，2－Bis（n－propylsulphinyl）ethane］－（O，O＇）－［diphenyltin（Ⅳ）dichloride］
    Yu Xi-Lin
    Bao Jian-Chun
    Shao Pin-Xi (Department of Chemistry
    Wang Hong-Gen
    Wang Ru-Ji(Central Laboratory
    结构化学, 1996, (01) : 20 - 23
  • [34] THE CRYSTAL AND MOLECULAR-STRUCTURE OF BIS[1,2-BIS(DIPHENYLPHOSPHINO)ETHANE]DICHLORORUTHENIUM(II)
    LOBANA, TS
    SINGH, R
    TIEKINK, ERT
    JOURNAL OF COORDINATION CHEMISTRY, 1990, 21 (03) : 225 - 229
  • [35] [1,2-Bis(1H-benzimidazol-2-yl-κN3)ethane]dichloridozinc(II)
    Zhou, Yan-Ling
    Zeng, Ming-Hua
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M57 - U640
  • [36] 3-Aminobenzoic acid-1,2-bis(4-pyridyl)ethane (1/1)
    Shen, Fwu Ming
    Lush, Shie Fu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1138 - U654
  • [37] COPPER(II) DERIVATIVES OF STEREOCHEMICALLY ADAPTIVE LIGANDS 1,2-BIS(2'-PYRIDYL)ETHANE AND BIS(2-PYRIDYL)DISULFIDE
    KEETON, M
    LEVER, ABP
    RAMASWAM.BS
    CANADIAN JOURNAL OF CHEMISTRY, 1970, 48 (20): : 3185 - &
  • [38] CRYSTAL-STRUCTURES OF 2 FORMS OF 1,2-BIS(DIPHENYLPHOSPHINO)ETHANE
    PELIZZI, C
    PELIZZI, G
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1979, 35 (AUG): : 1785 - 1790
  • [39] Crystal structure of bis{catena-poly[(μ2-1,2-bis(4-pyridyl)ethane-κ2N:N′)silver(I)]) diaqua-bis(5-(4-carboxyphenyl)pyridine-2-carboxylato-κ2N,O)-(μ2-1,2-bis(4-pyridyl)ethane-κ2N:N′)disilver(I) octahydrate, C31H35Ag2N4O9
    Fan, Hui-Tao
    Ding, Jie
    Xie, Jing-Peng
    Wang, Kun
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2018, 233 (04): : 585 - 587
  • [40] THE CRYSTAL AND MOLECULAR-STRUCTURE OF THE MESOGENIC 1,2-BIS (4'-PENTYLCYCLOHEXYL) ETHANE
    WALZ, L
    HAASE, W
    MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 1986, 4 (02): : 53 - 61
12345