Crystal Structure of 1,2-Bis[N,N '-6-(3-pyridylmethylamido)pyridyl-2-carboxy-amido]ethane

被引：1
|
作者：
Kadir, Maisara Abdul [1 ]
Yusof, M. Sukeri M. [1 ]
Sumby, C. J. [2 ]
机构：
[1] Univ Malaysia Terengganu, Sch Fundamental Sci, Kuala Nerus 21030, Terengganu, Malaysia
[2] Univ Adelaide, Sch Phys Sci, Ctr Adv Nanomat, Adelaide, SA 5005, Australia
来源：
X-RAY STRUCTURE ANALYSIS ONLINE | 2018年 / 34卷
关键词：
D O I：
10.2116/xraystruct.34.31
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
Compound 1, namely 1,2-bis[N,N'-6-(3-pyridylmethylamido)pyridyl-2-carboxyamido]ethane, crystallizes in the space group C2/c, with cell parameters a = 13.669(6)angstrom, b = 17.763(7)angstrom, c = 11.013(4)angstrom, beta = 108.857(16), Z = 4, and V = 2530.5(17)angstrom(3). The asymmetric unit comprises half of the title compound with the compound adopting a U-shaped conformation stabilized by intramolecular hydrogen bonding. Crystal packing is governed by N-H center dot center dot center dot N and C-H center dot center dot center dot O hydrogen bonds. The structure has been solved and refined to reach R and wR indices for all data of 0.0514 and 0.1366, respectively.
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页码：31 / 32
页数：2
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