STRUCTURE OF 1,3-BIS(TRIMETHYLSILYL)-2,4-BIS(TRIMETHYLSILYLAMINO)-2,4-DITHIOXOCYCLODI-LAMBDA-5-PHOSPHAZANE, [ME3SINHP(S)NSIME3]2

被引:5
作者
ZAK, Z [1 ]
GLOWIAK, T [1 ]
机构
[1] WROCLAW B BEIRUT UNIV, INST CHEM, PL-50383 WROCLAW, POLAND
来源
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 1991年 / 47卷
关键词
D O I
10.1107/S0108270190006424
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
[(CH3)3SiNHP(S)NSi(CH3)3]2, M(r) = 476.88, monoclinic, P2(1)/n, a = 13.587 (4), b = 6.634 (2), c = 15.328 (4) angstrom, beta = 99.82 (2)-degrees, V = 1361.4 (7) angstrom 3, Z = 2, D(m) = 1.165 Mg m-3, Mo K-alphaBAR, lambda = 0.71073 angstrom, mu = 0.44 mm-1, F(000) = 512, T = 295 K, R = 0.036 for 2334 unique observed reflections. The structure is composed of isolated molecules situated on centres of symmetry. The molecules are arranged in layers and held together by weak intermolecular forces as demonstrated macroscopically by a softness and plasticity of the crystals.
引用
收藏
页码:445 / 446
页数:2
相关论文
共 5 条
[1]   ON THE REACTION OF THIOPHOSPHORYL CHLORIDE WITH HEXAMETHYL DISILAZANE [J].
DOSTAL, K ;
SIKOLA, J ;
MEISEL, M ;
GRUNZE, H .
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1986, 543 (12) :199-206
[2]   SYNTHETIC, NMR SPECTROSCOPIC AND X-RAY CRYSTALLOGRAPHIC INVESTIGATIONS ON THE PRODUCTS OF THE REACTIONS OF PHENYL (METHYL) PHOSPHONOTHIOIC DICHLORIDE AND THIOPHOSPHORYL CHLORIDE AND PSCL3 WITH PRIMARY AMINES [J].
HURSTHOUSE, MB ;
IBRAHIM, EH ;
PARKES, HG ;
SHAW, LS ;
SHAW, RA ;
WATKINS, DA .
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1986, 28 (1-2) :261-266
[3]   THE STRUCTURES AND MODE OF FORMATION OF SOME CYCLODIPHOSPH(V) AZANES AND THEIR CIS-TRANS ISOMERIZATION [J].
HURSTHOUSE, MB ;
PARKES, HG ;
SHAW, LS ;
SHAW, RA ;
WATKINS, DA .
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1986, 28 (1-2) :221-227
[4]   PHOSPHAZENES AND PHOSPHAZANES [J].
SHAW, RA .
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1978, 4 (01) :101-121
[5]  
1971, XTL STRUCTURE DETERM