DETERMINATION OF AMINOCARB IN WATER BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引：10
|
作者：
BRUN, GL
MACDONALD, RM
机构：
[1] Inland Waters Direct., Dept. Environm., Moncton, N.B. E1C 8N6, Canada
来源：
BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY | 1980年 / 24卷 / 06期
关键词：
INSECTICIDES - Environmental Impact - WATER POLLUTION - Monitoring;
D O I：
10.1007/BF01608207
中图分类号：
X [环境科学、安全科学];
学科分类号：
08 ; 0830 ;
摘要：
Aminocarb (4-dimethylamino-3-methylphenyl N-methylcarbamate) is a carbamate insecticide that has been used extensively in eastern Canada to control forest infestation by the spruce budworm. The direct analysis of carbamate insecticides by gas liquid chromatography (GLC) is deemed difficult because of on-column instability at normal operating temperatures. In view of the inherent difficulties with GLC analysis, high performance liquid chromatography (HPLC) is a promising alternative. This paper describes the analysis of aminocarb by reverse phase HPLC using ultraviolet absorbance in series with fluorescence detection. A pre-concentration technique using Amberlite XAD-4 resin for the analysis of rain water is also elaborated. Refs.
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页码：886 / 893
页数：8
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