OXO-TRICYANO COMPLEXES OF MOLYBDENUM(IV) AND TUNGSTEN(IV) WITH BIDENTATE SCHIFF-BASES

被引：0
|
作者：
BURDA, B
BURGESS, J
PARSONS, SA
SAMOTUS, A
SZKLARZEWICZ, J
机构：
[1] JAGIELLONIAN UNIV,FAC CHEM,PL-30060 KRAKOW,POLAND
[2] UNIV LEICESTER,DEPT CHEM,LEICESTER LE1 7RH,LEICS,ENGLAND
来源：
TRANSITION METAL CHEMISTRY | 1995年 / 20卷 / 03期
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D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The reaction of [M(CN)(4)O(OH2)](2-) (M = Mo or W) with 2-acetylpyridine and methyl- or butyl-amine in a water-MeOH mixture gave [M(CN)(3)O(L-L)](-) (L-L = Schiff base ligand), isolated as [AsPh(4)](+) salts. The complexes have been characterized by elemental analysis, and electronic, i.r. and H-1-n.m.r. spectroscopy. The Schiff base ligands complex in a bidentate manner through the two nitrogen atoms giving mixed-ligand compounds similarly to 2,2'-bipyridyl or 1,10-phenanthroline.
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页码：291 / 294
页数：4
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