SOLID-STATE PROTON MULTIPLE-QUANTUM NMR-SPECTROSCOPY WITH FAST MAGIC-ANGLE-SPINNING

被引：122
|
作者：
GEEN, H
TITMAN, JJ
GOTTWALD, J
SPIESS, HW
机构：
[1] Max-Planck-Institut für Polymerforschung, D-55021 Mainz
来源：
CHEMICAL PHYSICS LETTERS | 1994年 / 227卷 / 1-2期
关键词：
D O I：
10.1016/0009-2614(94)00789-6
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
The feasibility of multiple-quantum NMR spectroscopy with high resolution for protons in solids is explored. A new multiple-quantum excitation sequence suitable for use with fast magic angle spinning is described, and its performance is compared to that of both static and slow-spinning multiple-quantum methods. Modified sequences which scale the rate of development of the multiple-quantum coherences are also demonstrated, and two-dimensional double-quantum spectra of adamantane and polycarbonate are presented.
引用
收藏
页码：79 / 86
页数：8
相关论文
共 50 条
  • [31] Proton-Detected Solid-State NMR Spectroscopy of Bone with Ultrafast Magic Angle Spinning
    Mroue, Kamal H.
    Nishiyama, Yusuke
    Pandey, Manoj Kumar
    Gong, Bo
    McNerny, Erin
    Kohn, David H.
    Morris, Michael D.
    Ramamoorthy, Ayyalusamy
    SCIENTIFIC REPORTS, 2015, 5
  • [32] Multiple-quantum magic-angle spinning and dynamic-angle spinning NMR spectroscopy of quadrupolar nuclei
    Wang, SH
    Xu, Z
    Baltisberger, JH
    Bull, LM
    Stebbins, JF
    Pines, A
    SOLID STATE NUCLEAR MAGNETIC RESONANCE, 1997, 8 (01) : 1 - 16
  • [33] Paramagnetic Solid-State Magic-Angle Spinning NMR Spectroscopy
    Pintacuda, Guido
    Kervern, Gwendal
    MODERN NMR METHODOLOGY, 2013, 335 : 157 - 200
  • [34] Heteronuclear recoupling in solid-state magic-angle-spinning NMR via overtone irradiation
    Wi, SS
    Frydman, L
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2001, 123 (42) : 10354 - 10361
  • [35] Fullerene as a standard sample for adjusting the NMR spectral resolution in multiple-quantum magic-angle-spinning experiments
    Shimoikeda, Yuichi
    Utsumi, Hiroaki
    Saito, Koji
    Shimizu, Tadashi
    Nakai, Toshihito
    ANALYTICAL SCIENCES, 2007, 23 (08) : 1007 - 1009
  • [36] Decoupling-induced recoupling in multiple-quantum magic-angle-spinning NMR spectra of quadrupolar nuclei
    Wu, G
    CHEMICAL PHYSICS LETTERS, 2000, 322 (06) : 513 - 519
  • [37] Fullerene as a Standard Sample for Adjusting the NMR Spectral Resolution in Multiple-Quantum Magic-Angle-Spinning Experiments
    Yuichi Shimoikeda
    Hiroaki Utsumi
    Koji Saito
    Tadashi Shimizu
    Toshihito Nakai
    Analytical Sciences, 2007, 23 : 1007 - 1009
  • [38] Observation of 1H-1H J-couplings in fast magic-angle-spinning solid-state NMR spectroscopy
    Torodii, Daria
    Holmes, Jacob B.
    Grohe, Kristof
    de Oliveira-Silva, Rodrigo
    Wegner, Sebastian
    Sakellariou, Dimitrios
    Emsley, Lyndon
    NATURE COMMUNICATIONS, 2024, 15 (01)
  • [39] HIGH-RESOLUTION MAGIC ANGLE SPINNING AND CROSS-POLARIZATION MAGIC ANGLE SPINNING SOLID-STATE NMR-SPECTROSCOPY - ANALYTICAL CHEMICAL APPLICATIONS
    FYFE, CA
    BEMI, L
    CLARK, HC
    DAVIES, JA
    GOBBI, GC
    HARTMAN, JS
    HAYES, PJ
    WASYLISHEN, RE
    ACS SYMPOSIUM SERIES, 1983, 211 : 405 - 430
  • [40] CROSS POLARIZATION MAGIC ANGLE SPINNING PROTON NMR-SPECTROSCOPY OF SOLIDS
    CROSBY, RC
    REESE, RL
    HAW, JF
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1988, 110 (25) : 8550 - 8551
12345