SOLID-STATE PROTON MULTIPLE-QUANTUM NMR-SPECTROSCOPY WITH FAST MAGIC-ANGLE-SPINNING

被引：122
|
作者：
GEEN, H
TITMAN, JJ
GOTTWALD, J
SPIESS, HW
机构：
[1] Max-Planck-Institut für Polymerforschung, D-55021 Mainz
来源：
CHEMICAL PHYSICS LETTERS | 1994年 / 227卷 / 1-2期
关键词：
D O I：
10.1016/0009-2614(94)00789-6
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
The feasibility of multiple-quantum NMR spectroscopy with high resolution for protons in solids is explored. A new multiple-quantum excitation sequence suitable for use with fast magic angle spinning is described, and its performance is compared to that of both static and slow-spinning multiple-quantum methods. Modified sequences which scale the rate of development of the multiple-quantum coherences are also demonstrated, and two-dimensional double-quantum spectra of adamantane and polycarbonate are presented.
引用
收藏
页码：79 / 86
页数：8
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