OPTIMIZATION OF EXTRACTION PROCEDURE FOR DETERMINATION OF TOTAL WATER-SOLUBLE CHROMIUM AND CHROMIUM(VI) IN VARIOUS SOILS

被引:13
作者
KOZUH, N [1 ]
STUPAR, J [1 ]
MILACIC, R [1 ]
GORENC, B [1 ]
机构
[1] UNIV LJUBLJANA, DEPT CHEM & CHEM TECHNOL, LJUBLJANA 61000, SLOVENIA
关键词
CHROMIUM; CHROMIUM(VI); CHELATING ION-EXCHANGE CHROMATOGRAPHY; ELECTROTHERMAL AAS; EXTRACTION PROCEDURE; SOIL EXTRACTS;
D O I
10.1080/03067319408034101
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The parameters influencing the extraction efficiency of total water-soluble chromium and chromium(VI) in clay, peat and sandy soils were investigated. Water and a KH2 PO4 solution (0.015 mol dm(-3)) were used as extractants. Samples were ultrasonicated or shaken in classical shakers. Variations of solution volume-to-soil weight ratio, and of shaking time were studied in order to develop the optimal extraction procedure for the determination of total water-soluble chromium and chromium(VI). Soil samples treated with tannery waste continuously for 17 years and soils freshly contaminated with the same waste were studied.
引用
收藏
页码:207 / 217
页数:11
相关论文
共 50 条
  • [21] Spectrophotometric determination of chromium(VI) by extraction of the dichromate anion into propylene carbonate
    Burns, DT
    Dangolle, CDF
    ANALYTICA CHIMICA ACTA, 1997, 356 (2-3) : 145 - 148
  • [22] Application of Test Kits for Water Samples to Screening Contaminated Soils for Chromium (VI)
    Sakai, Hiroyuki
    Imai, Kazumichi
    Suzuki, Yoshihiro
    Wada, Shin-Ichiro
    JOURNAL OF THE FACULTY OF AGRICULTURE KYUSHU UNIVERSITY, 2012, 57 (02): : 481 - 483
  • [23] Sensitive and selective spectrofluorimetric determination of chromium(VI) in water by fluorescence enhancement
    Xiang, Yu
    Mei, Ling
    Li, Na
    Tong, Aijun
    ANALYTICA CHIMICA ACTA, 2007, 581 (01) : 132 - 136
  • [24] Determination of Chromium(VI) in waste water by Reversed Flow Injection Spectrophotometry
    Su, Ling
    Xie, Hengshen
    PROGRESS IN ENVIRONMENTAL SCIENCE AND ENGINEERING (ICEESD2011), PTS 1-5, 2012, 356-360 : 939 - 942
  • [25] Field determination of leachable chromium(VI) in soil by ultrasonic extraction - Diphenylcarbazide colorimetry
    Kawakubo, Susumu
    Suzuki, Yasutada
    Yamanoi, Takashi
    Maruta, Toshihisa
    Nagase, Takahiro
    BUNSEKI KAGAKU, 2007, 56 (04) : 231 - 235
  • [26] FLOW-INJECTION EXTRACTION SPECTROPHOTOMETRIC DETERMINATION OF CHROMIUM(VI) WITH THE BENZYLTRIBUTYLAMMONIUM CATION
    BARAKAT, SA
    BURNS, DT
    HARRIOTT, M
    ANALYTICA CHIMICA ACTA, 1993, 272 (01) : 135 - 138
  • [27] Application of an optimization procedure in adsorptive stripping voltammetry for the determination of chromium with diphenylcarbazide
    Domínguez, O
    Sanllorente, S
    Arcos, MJ
    QUIMICA ANALITICA, 1999, 18 (01): : 143 - 149
  • [28] Application of an optimization procedure of adsorptive stripping voltammetry for the determination of chromium in wine
    Dominguez, O
    Sanllorente, S
    Arcos, MJ
    ELECTROANALYSIS, 1999, 11 (17) : 1273 - 1279
  • [29] Leaching Properties of Water-Soluble Hexavalent Chromium by Manufacturing Condition of Cement Clinker
    Lee, Jong-Kyu
    Chu, Yong-Sik
    Song, Hun
    KOREAN JOURNAL OF MATERIALS RESEARCH, 2011, 21 (12): : 679 - 684
  • [30] Ion chromatography method for the determination of trace levels of chromium(VI) in water
    Michalski, R
    POLISH JOURNAL OF ENVIRONMENTAL STUDIES, 2004, 13 (01): : 73 - 77