OPTIMIZATION OF EXTRACTION PROCEDURE FOR DETERMINATION OF TOTAL WATER-SOLUBLE CHROMIUM AND CHROMIUM(VI) IN VARIOUS SOILS

被引：13

作者：

KOZUH, N ^{[1
]}

STUPAR, J ^{[1
]}

MILACIC, R ^{[1
]}

GORENC, B ^{[1
]}

机构：

[1] UNIV LJUBLJANA, DEPT CHEM & CHEM TECHNOL, LJUBLJANA 61000, SLOVENIA

来源：

INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY | 1994年 / 56卷 / 03期

关键词：

CHROMIUM; CHROMIUM(VI); CHELATING ION-EXCHANGE CHROMATOGRAPHY; ELECTROTHERMAL AAS; EXTRACTION PROCEDURE; SOIL EXTRACTS;

D O I：

10.1080/03067319408034101

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The parameters influencing the extraction efficiency of total water-soluble chromium and chromium(VI) in clay, peat and sandy soils were investigated. Water and a KH2 PO4 solution (0.015 mol dm(-3)) were used as extractants. Samples were ultrasonicated or shaken in classical shakers. Variations of solution volume-to-soil weight ratio, and of shaking time were studied in order to develop the optimal extraction procedure for the determination of total water-soluble chromium and chromium(VI). Soil samples treated with tannery waste continuously for 17 years and soils freshly contaminated with the same waste were studied.

引用

页码：207 / 217

页数：11

共 17 条

[1] BEHAVIOR OF CHROMIUM IN SOILS .3. OXIDATION [J].

BARTLETT, R ;

JAMES, B .

JOURNAL OF ENVIRONMENTAL QUALITY, 1979, 8 (01) :31-35

[2] CHEMICAL-EXTRACTION OF HEAVY-METALS IN POLLUTED RIVER SEDIMENTS IN CENTRAL-EUROPE [J].

CALMANO, W ;

FORSTNER, U .

SCIENCE OF THE TOTAL ENVIRONMENT, 1983, 28 (JUN) :77-90

[3] SOLID-PHASE FORMS OF HEAVY-METALS IN SEWAGE SLUDGE-TREATED SOILS [J].

EMMERICH, WE ;

LUND, LJ ;

PAGE, AL ;

CHANG, AC .

JOURNAL OF ENVIRONMENTAL QUALITY, 1982, 11 (02) :178-181

[4] EXTRACTABLE CHROMIUM AS RELATED TO SOIL-PH AND APPLIED CHROMIUM [J].

GROVE, JH ;

ELLIS, BG .

SOIL SCIENCE SOCIETY OF AMERICA JOURNAL, 1980, 44 (02) :238-242

[5] AN ATOMIC-ABSORPTION SPECTROMETRIC METHOD FOR THE INDIVIDUAL DETERMINATION OF CHROMIUM(III) AND CHROMIUM(VI) BY ATOMIZATION OF CHROMIUM FROM A CHELATING RESIN IN A GRAPHITE TUBE [J].

ISOZAKI, A ;

KUMAGAI, K ;

UTSUMI, S .

ANALYTICA CHIMICA ACTA, 1983, 153 (OCT) :15-22

[6]

JAMES B, 1983, J ENVIRON QUAL, V12, P117

[7] BEHAVIOR OF CHROMIUM IN SOILS .6. INTERACTIONS BETWEEN OXIDATION-REDUCTION AND ORGANIC COMPLEXATION [J].

JAMES, BR ;

BARTLETT, RJ .

JOURNAL OF ENVIRONMENTAL QUALITY, 1983, 12 (02) :173-176

[8] ACCURACY OF SELECTIVE EXTRACTION PROCEDURES FOR METAL SPECIATION IN MODEL AQUATIC SEDIMENTS [J].

KHEBOIAN, C ;

BAUER, CF .

ANALYTICAL CHEMISTRY, 1987, 59 (10) :1417-1423

[9] FRACTIONATION, CHARACTERIZATION, AND SPECIATION OF HEAVY-METALS IN SEWAGE-SLUDGE AND SLUDGE-AMENDED SOILS - A REVIEW [J].

LAKE, DL ;

KIRK, PWW ;

LESTER, JN .

JOURNAL OF ENVIRONMENTAL QUALITY, 1984, 13 (02) :175-183

[10] IDENTIFICATION OF COPPER CONTAMINATION IN SEDIMENTS BY A MICROSCALE PARTIAL EXTRACTION TECHNIQUE [J].

MESUERE, K ;

MARTIN, RE ;

FISH, W .

JOURNAL OF ENVIRONMENTAL QUALITY, 1991, 20 (01) :114-118

← 1 2 →