2-[(E)-(4-Fluorobenzyl)iminomethyl]6-methoxyphenol

被引:0
作者
Yu, Hong [1 ]
Jin, Yue-Bao [1 ]
Chang, Yong-Kang [1 ]
Lei, Ke-Wei [1 ]
机构
[1] Ningbo Univ, Fac Mat Sci & Chem Engn, Inst Solid Mat Chem, State Key Lab Base Novel Funct Mat & Preparat Sci, Ningbo 315211, Zhejiang, Peoples R China
关键词
data-to-parameter ratio = 9.7; mean σ(C-C) = 0.005 Å; R factor = 0.042; single-crystal X-ray study; T = 293 K; wR factor = 0.125;
D O I
10.1107/S1600536812027419
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title Schiff base, C15H14FNO2, the dihedral angle between the benzene rings is 53.32 (8)degrees. In the crystal, molecules related by a twofold rotation axis are linked by pairs of C-H center dot center dot center dot O hydrogen bonds into dimers with R-2(2) (18) ring motifs. An intramolecular O-H center dot center dot center dot N hydrogen bond is also observed.
引用
收藏
页码:02401 / +
页数:6
相关论文
共 6 条
[1]   TOPOCHEMISTRY .6. EXPERIMENTS ON PHOTOCHROMY + THERMOCHROMY OF CRYSTALLINE ANILS OF SALICYLALDEHYDES [J].
COHEN, MD ;
SCHMIDT, GMJ ;
FLAVIAN, S .
JOURNAL OF THE CHEMICAL SOCIETY, 1964, (JUN) :2041-&
[2]  
Higashi, 1995, ABSCOR PROGRAM ABSOR
[3]   2-(Benzyliminomethyl)-6-methoxyphenol [J].
Li, Zhong-Fang ;
Wang, Su-Wen ;
Zhang, Qian ;
Yu, Xian-Jin .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 :O3930-U1884
[4]  
*RIG CORP, 1998, RAPID AUTO
[5]  
*RIG MSC INC, 2004, CRYSTALSTRUCTURE
[6]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122