2,6-Bis[(S)-1-phenylethyl]-1H,5H-pyrrolo[3,4-f] isoindole-1,3,5,7(2H, 6H)-tetrone

被引：0

作者：

Abdel-Aziz, Alaa A. -M. ^{[1
,2
]}

El-Azab, Adel S. ^{[1
,3
]}

Alanazi, Amer M. ^{[1
]}

Ng, Seik Weng ^{[4
,5
]}

Tiekink, Edward R. T. ^{[4
]}

机构：

[1] King Saud Univ, Coll Pharm, Dept Pharmaceut Chem, Riyadh 11451, Saudi Arabia

[2] Univ Mansoura, Fac Pharm, Dept Med Chem, Mansoura 35516, Egypt

[3] Al Azhar Univ, Fac Pharm, Dept Organ Chem, Cairo 11884, Egypt

[4] Univ Malaya, Dept Chem, Kuala Lumpur 50603, Malaysia

[5] King Abdulaziz Univ, Fac Sci, Chem Dept, Jeddah, Saudi Arabia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-to-parameter ratio = 14.2; mean σ(C-C) = 0.002 Å; R factor = 0.033; single-crystal X-ray study; T = 100 K; wR factor = 0.099;

D O I：

10.1107/S1600536812007684

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C 26H 20N 2O 4, the central isoindole core is almost planar (r.m.s. deviation = 0.043 Å). The phenyl rings lie to either side of the plane [dihedral angles = 88.64 (5) and 67.74 (6)°] and the dihedral angle between the phenyl rings is 63.39 (7)°. In the crystal, mol-ecules are linked by C - H⋯O interactions; notably, one carbonyl O atom accepts three such bonds.

引用

页码：O907 / U3544

页数：10

共 50 条

[41] 3-Ethyl-4-methyl-1H-pyrazol-2-ium-5-olate [J].

Rathore, R. S. ;

Narasimhamurthy, T. ;

Ragavan, R. Venkat ;

Vijayakumar, V. ;

Sarveswari, S. .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O2129-U1355

[42] 3-(2,3,5,6,7,8-Hexahydro-1H-cyclopenta[b]quinolin-9-yl)-1,5-bis(4-methoxyphenyl)biuret [J].

Sakurai, Kaori ;

Noguchi, Keiichi ;

Nishibe, Koichiro .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O655-U5355

[43] Ethyl (1R,1′S,2′S,7a′R)-2-oxo-1′-[(3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyltetrahydro-3aH-bis[1,3]dioxolo[4,5-b:4′,5′-d]pyran-5-yl]-1′,2′,5′,6′,7′,7a′-hexahydro-2H-spiro[acenaphthylene-1,3′-pyrrolizine]-2′-carboxylate [J].

Jagadeesan, G. ;

Sethusankar, K. ;

Prasanna, R. ;

Raghunathan, R. .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 :O382-U470

[44] 1,3-Bis[2-hydroxy-2-(6-methoxy-2,2-dimethyl-3a,5,6,6a-tetrahydro-2H-furo[2,3-d][1,3]dioxol-5-yl)ethyl]-2,3-dihydro-1H-1,3-benzodiazol-2-one [J].

Lakhrissi, Brahim ;

Massoui, Mohamed ;

Ramli, Youssef ;

Essassi, El Mokhtar ;

Ng, Seik Weng .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 :O351-U188

[45] 6,7-Dichloro-3-(2,4-dichlorobenzyl)quinoxalin- 2(1H)-one [J].

Zhang, Jinpeng ;

Wang, Yinan ;

Wang, Qian ;

Xu, Lichun .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :02481-+

[46] Chlorido[5-methoxy-1H-benzimidazole2-(3H)-thione-kappa S] bis(triphenylphosphane-kappa P) copper(I) methanol disolvate [J].

Meng, Qing-Xuan .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 :M60-+

[47] Bis[2,3,4-trimethyl-5-[(3,4,5-trimethyl-2H-pyrrol-2-ylidene-kappa N) methyl]-1H-pyrrolato- kappa N] copper(II) [J].

Erdem, Sultan S. ;

Fronczek, Frank R. ;

Watkins, Steven F. .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :M1335-+

[48] N-[3-Cyano-2-oxo-5,6,7,8-tetrahydroquinoline-1(2H)-yl]-4-methylbenzenesulfonamide [J].

Elgemeie, GH ;

Jones, PG .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2002, 58 :O1250-O1252

[49] Ethyl 2-{5-[(3-oxo-3,4-dihydro-2H-1,4-benzothiazin-4-yl)methyl]-1H-1,2,3-triazol-1-yl}acetate [J].

Sebbar, Nada Kheira ;

Zerzouf, Abdelfettah ;

Essassi, El Mokhtar ;

Saadi, Mohamed ;

El Ammari, Lahcen .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 :0116-+

[50] Ethyl 4-(5-bromo-1H-indol-3-yl)-2,6,6-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate [J].

Gunduz, Miyase Gozde ;

Butcher, Ray J. ;

Yildirim, Sema Ozturk ;

El-Khouly, Ahmed ;

Safak, Cihat ;

Simsek, Rahime .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O3404-+

← 1 2 3 4 5 →