Crystal structure of 2,3-bis[(4-tert-butyl-2,6-dimethylphenyl)imino]butane

被引：0
|
作者：
Zhao, Sheng-Lan [1 ]
Yuan, Jian-Chao [1 ]
Zhao, Yan [1 ]
机构：
[1] Northwest Normal Univ, Key Lab Ecoenvironm Related Polymer Mat, Key Lab Polymer Mat Gansu Prov, Minist Educ,Coll Chem & Chem Engn, Lanzhou 730070, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2015年 / 71卷
基金：
中国国家自然科学基金;
关键词：
crystal structure; alpha-diimine ligand; catalyst; aniline; diimino-butane;
D O I：
10.1107/S2056989015005551
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C28H4ON2, was obtained from the condensation reaction of 4-tert-butyl-2,6-dimethylaniline and butane-2,3-dione. The molecule lies on an inversion centre. The C=N bond has an E conformation. The plane of the benzene ring is almost perpendicular to the 1,4-diazabutadiene mean plane [dihedral angle = 89.8 (9)degrees].
引用
收藏
页码：O258 / U388
页数：6
相关论文
共 50 条
  • [41] STRUCTURES OF 2-(2,6-DICHLOROPHENYL)IMINO-3-METHYLPERHYDRO-1,3-THIAZINE, 2-(2,6-DIMETHYLPHENYL)IMINO-3-METHYLPERHYDRO-1,3-THIAZINE AND 2-[N-(2,6-DIMETHYLPHENYL)-N-METHYLAMINO]-4,5-DIHYDRO-6H-1,3-THIAZINE
    ARGAY, G
    KALMAN, A
    KAPOR, A
    RIBAR, B
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 1980, 36 (FEB) : 363 - 368
  • [42] CRYSTAL AND MOLECULAR STRUCTURE OF PRIMARY OXIDATION PRODUCT OF S-(2-METHOXYPHENY1)-(-(2,6-DIMETHYLPHENYL)DITHIOURETHAN
    KATO, K
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL CRYSTALLOGRAPHY AND CRYSTAL CHEMISTRY, 1972, B 28 (SEP15): : 2653 - &
  • [43] Crystal structure of (E)-3-[(2,6-dimethylphenyl)-diazenyl]-7-methyl-1H-indazole
    Yagi, Shiomi
    Haraguchi, Tomoyuki
    Akitsu, Takashiro
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2018, 74 : 1421 - +
  • [44] 4-Fluoropyrrolidine-2-carbonyl Fluorides: Useful Synthons and Their Facile Preparation with 4-tert-Butyl-2,6-dimethylphenylsulfur Trifluoride
    Singh, Rajendra P.
    Umemoto, Teruo
    JOURNAL OF ORGANIC CHEMISTRY, 2011, 76 (09): : 3113 - 3121
  • [45] Synthesis, spectroscopic studies, and crystal structures of phenylorganotin derivatives with [bis(2,6-dimethylphenyl)amino]benzoic acid: Novel antituberculosis agents
    Dokorou, V
    Kovala-Demertzi, D
    Jasinski, JP
    Galani, A
    Demertzis, MA
    HELVETICA CHIMICA ACTA, 2004, 87 (08) : 1940 - 1950
  • [46] CRYSTAL-STRUCTURE AND PROPERTIES OF DIMETHYL 2,3-BIS(DIPHENYLPHOSPHINO)FUMARATE
    FENSKE, D
    LONS, J
    CHEMISCHE BERICHTE-RECUEIL, 1975, 108 (09): : 3091 - 3095
  • [47] catena-Poly[[[diaquacadmium(II)]-bis[μ-4-tert-butyl-2,6-bis(1,2,4-triazol-1-yl-methyl)phenol]] dinitrate dihydrate]
    Chu, Zhao-Lian
    Xu, Gang
    Huang, Wei
    Gou, Shao-Hua
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : M2155 - U1170
  • [48] Synthesis of 1,3-Bis(2,6-dimethylphenyl)-2-tetrahydroimidazol(C5H5N)2(Cl)2Ru=CHPh
    Bai, Chen-Xi
    Zhang, Wen-Zhen
    He, Ren
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2006, 26 (12) : 1700 - 1703
  • [49] Crystal structure of N-butyl-2,3-bis(dicyclohexyl-amino)cyclopropeniminium chloride benzene monosolvate
    Sanchez, Gaby M. Munoz
    Zdilla, Michael J.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2022, 78 : 936 - +
  • [50] A novel one-pot synthesis of symmetric dialkyl 2,5-bis((2,6-dimethylphenyl)imino)-2,5-dihydrofuran-3,4-dicarboxylate derivatives
    Maghsoodlou, Malek Taher
    Khandan-Barani, Khatereh
    Hazeri, Nourallah
    Habibi-Khorasani, Sayyed Mostafa
    Willis, Anthony C.
    RESEARCH ON CHEMICAL INTERMEDIATES, 2014, 40 (02) : 779 - 785
12345