5-Fluoro-3-phenyl-N '-(4-propylcyclohexylidene)-1H-indole-2-carbohydrazide

被引:1
作者
Celikesir, Sevim Turktekin [1 ]
Akkurt, Mehmet [1 ]
Ustundag, Gokce Cihan [2 ]
Buyukgngor, Orhan [3 ]
机构
[1] Erciyes Univ, Fac Sci, Dept Phys, TR-38039 Kayseri, Turkey
[2] Istanbul Univ, Fac Pharm, Dept Pharmaceut Chem, TR-34116 Istanbul, Turkey
[3] Ondokuz Mayis Univ, Fac Arts & Sci, Dept Phys, TR-55139 Samsun, Turkey
关键词
data-to-parameter ratio = 17.0; meanω(C - C) = 0.005 A °; Rfactor = 0.047; single-crystal X-ray study; T = 296 K; wRfactor = 0.092;
D O I
10.1107/S1600536813018333
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C24H26FN3O, the cyclohexane ring adopts a chair conformation; the propyl substituent is in an equatorial orientation and the bond-angle sum at the C atom bonded to the carbohydrazide N atom is 360.0 degrees. The dihedral angle between the 1H-indole ring system and the phenyl ring is 82.77 (13)degrees . A weak intramolecular C-H center dot center dot center dot pi contact occurs. In the crystal, pairs of molecules related by a crystallographic twofold axis are linked by bifurcated N-H center dot center dot center dot (O, N) hydrogen bonds; a C-H center dot center dot center dot O interaction occurs between the same pair. The dimers are linked by C-H center dot center dot center dot F and C-H center dot center dot center dot pi interactions, generating a three- dimensional network.
引用
收藏
页码:O1202 / +
页数:9
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