N-(2-Chloro-5-nitrophenyl)-N '-(3-chloropropionyl)thiourea

被引:0
作者
Yamin, Bohari M. [1 ]
Soh, Siti K. C. [1 ]
Yusoff, Siti Fairus M. [1 ]
机构
[1] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Bangi 43600, Selangor, Malaysia
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷
关键词
D O I
10.1107/S1600536813032662
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C10H9Cl2N3O3S, adopts a trans-cis conformation with respect to the position of chloropropionyl and chloronitrobenzene groups respectively, against the thiono about their C-N bonds. The conformation is stabilized by an intramolecular N-H center dot center dot center dot O hydrogen bond. In the crystal, there is a short Cl center dot center dot center dot Cl contact with a distance of 3.386 (13) angstrom.
引用
收藏
页码:O34 / +
页数:6
相关论文
共 7 条
[1]  
Bruker, 2000, SMART SAINT SADABS
[2]   N-(3-Chloropropionyl)-N′-phenylthiourea [J].
Othman, Eliyanti A. ;
Soh, Siti K. C. ;
Yamin, Bohari M. .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O628-U5121
[3]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[4]   Structure validation in chemical crystallography [J].
Spek, Anthony L. .
ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 :148-155
[5]   N-(4-Bromobutanoyl)-N′-phenylthiourea [J].
Yamin, Bohari M. ;
Othman, Nur Eliyanti Ali .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O1629-U182
[6]   N-(4-Chlorobutanoyl)-N′-phenylthiourea [J].
Yamin, Bohari M. ;
Othman, Nur Eliyanti Ali ;
Yusof, M. Sukeri M. ;
Embong, Farhana .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O419-U1112
[7]   N-(4-Chlorobutanoyl)-N′-(2-fluorophenyl)thiourea [J].
Yusof, M. Sukeri M. ;
Embong, Nur Farhana ;
Othman, Eliyanti A. ;
Yamin, Bohari M. .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O1849-U2082