COMPARATIVE STUDY OF ADSORPTION ISOTHERMS AND GAS-CHROMATOGRAPHIC PROPERTIES OF POWDERED ETCHED GLASS

被引:9
作者
ALBERINI, G
BRUNER, F
DEVITOFR.G
机构
[1] Istituto di Chimica Analitica, Universita di Roma, 00185 Roma, Italy
关键词
D O I
10.1021/ac50159a025
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The continuous flow system is used to determine the nitrogen adsorption isotherms of glass powders etched with hot alkaline solutions. The effect of alkali concentration on surface area, isotherm shape and pore volume distribution is compared with the gas-chromatographic properties of the glass powder. Etching conditions are found to be critical. Water vapour is used as surface deactivant and its effect on surface characteristics is related to the change on retention volumes and column efficiency. © 1969, American Chemical Society. All rights reserved.
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页码:1940 / &
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