REACTION OF NIOBIUM PENTACHLORIDE WITH BIS(TRIETHYLGERMYL)CADMIUM

被引：0

作者：

LOMAKOVA, IV

DOMRACHEV, GA

PATRIKEEVA, NB

PETROV, BI

机构：

[1] Institute of Organometallic Chemistry, Russian Academy of Sciences, Nizhnii Novgorod, 603600

来源：

RUSSIAN CHEMICAL BULLETIN | 1994年 / 43卷 / 10期

关键词：

NIOBIUM PENTACHLORIDE; REACTION WITH BIS(TRIETHYLGERMYL)CADMIUM TRIETHYLGERMYLNIOBIUM PENTACHLORIDE; MONOSOLVATE WITH THF; THERMOLYSIS; VOLATILE AND SOLID PRODUCTS;

D O I：

10.1007/BF00703496

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The reaction of niobium pentachloride with Cd(GeEt(3))(2) (1 : 1) in THF in vacuo has been studied. The reaction affords Et(3)GeNbCl(4) . THF, which was characterized by elemental analysis and IR spectroscopy. To refine the composition of the compound, the thermolysis of Et(3)GeNbCl(4) . THF at 85 and 180 degrees C was studied.

引用

页码：1717 / 1718

页数：2

共 32 条

[31] Reaction of bis(dimethoxyphosphino)dimethylhydrazine (dmpdmh) with Ru3(CO)12: Evidence for facile ligand fragmentation in Ru3(CO)10(dmpdmh) to give Ru4(CO)12[μ-N(Me)N(Me)], Ru3(CO)11[P(OMe)3], and Ru3(CO)9[μ-P(OMe)3]
Simon G. Bott
Jian Cheng Wang
Michael G. Richmond
Journal of Chemical Crystallography, 1999, 29 : 587 - 595
[32] Reaction of bis(dimethoxyphosphino)dimethylhydrazine (dmpdmh) with Ru3(CO)12:: Evidence for facile ligand fragmentation in Ru3(CO)10(dmpdmh) to give Ru4(CO)12[μ-N(Me)N(Me)], Ru3(CO)11[P(OMe)3], and Ru3(CO)9[μ-P(OMe)3]
Bott, SG
Wang, JC
Richmond, MG
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 1999, 29 (05) : 587 - 595

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