REACTION OF NIOBIUM PENTACHLORIDE WITH BIS(TRIETHYLGERMYL)CADMIUM

被引：0
|
作者：
LOMAKOVA, IV
DOMRACHEV, GA
PATRIKEEVA, NB
PETROV, BI
机构：
[1] Institute of Organometallic Chemistry, Russian Academy of Sciences, Nizhnii Novgorod, 603600
来源：
RUSSIAN CHEMICAL BULLETIN | 1994年 / 43卷 / 10期
关键词：
NIOBIUM PENTACHLORIDE; REACTION WITH BIS(TRIETHYLGERMYL)CADMIUM TRIETHYLGERMYLNIOBIUM PENTACHLORIDE; MONOSOLVATE WITH THF; THERMOLYSIS; VOLATILE AND SOLID PRODUCTS;
D O I：
10.1007/BF00703496
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The reaction of niobium pentachloride with Cd(GeEt(3))(2) (1 : 1) in THF in vacuo has been studied. The reaction affords Et(3)GeNbCl(4) . THF, which was characterized by elemental analysis and IR spectroscopy. To refine the composition of the compound, the thermolysis of Et(3)GeNbCl(4) . THF at 85 and 180 degrees C was studied.
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收藏
页码：1717 / 1718
页数：2
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