1,1,2,2,3,3,4,4,5,5,6,6-DODECAMETHYL-1,2,4,5-TETRASTANNACYCLOHEXANE

被引：3
作者：
PREUT, H
MITCHELL, TN
机构：
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1991年 / 47卷
关键词：
D O I：
10.1107/S010827019001232X
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
C14H36Sn4, M(r) = 679.20, monoclinic, P2(1)/n, a = 8.236 (3), b = 13.584 (5), c = 10.738 (3) angstrom, beta = 94.27 (3)-degrees, V = 1198.0 (7) angstrom 3, Z = 2, D(x) = 1.883 Mg m-3, lambda(Mo K-alpha) = 0.71073 angstrom, mu = 4.13 mm-1, F(000) = 640, T = 291 (1) K, final R = 0.028 for 1999 unique observed [F greater-than-or-equal-to 3.0-sigma(F)] diffractometer data. In the crystal the molecule resides on a centre of symmetry. The central 1,2,4,5-tetrastanna-cyclohexane ring has a chair conformation with an Sn-Sn bond length of 2.7753 (8) angstrom. The structure consists of discrete molecular units.
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页码：951 / 953
页数：3
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