Efficiency of QuEChERS approach for determining 52 pesticide residues in honey and honey bees

被引:66
作者
Calatayud-Vernich, Pau [1 ]
Calatayud, Fernando [2 ]
Simo, Enrique [2 ]
Pico, Yolanda [1 ]
机构
[1] Univ Valencia, Res Ctr Desertificat CIDE, UV CSIC GV, Environm & Food Safety Res Grp SAMA UV,Fac Pharm, Ave Vicent Andres Estelles S-N, E-46100 Valencia, Spain
[2] Agrupac Def Sanitaria Apicola ApiADS, Ctra Montroi Turis, Valencia 46193, Spain
来源
METHODSX | 2016年 / 3卷
关键词
QuEChERS; solid phase extraction (SPE); solvent extraction; honey; honey bee; pesticide; LC-MS/MS;
D O I
10.1016/j.mex.2016.05.005
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
A comparison between QuEChERS and other pesticide extraction procedures for honey and honey bee matrices is discussed. Honey bee matrix was extracted by solvent based procedure whereas solid phase extraction was the protocol for the honey matrix. The citrate buffered QuEChERS method was used for both matrices. The methods were evaluated regarding cost (equipment and reagents), time, accuracy, precision, sensitivity and versatility. The results proved that the QuEChERS protocol was the most efficient method for the extraction of the selected pesticides in both matrices. QuEChERS is the most economical and less time-consuming procedure. SPE and solvent-based extraction procedures show equivalent recoveries to QuEChERS. QuEChERS can be used to extract pesticide residues from both matrices. (C) 2016 The Authors. Published by Elsevier B.V. This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).
引用
收藏
页码:452 / 458
页数:7
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