SYNTHESIS AND PROPERTIES OF A ZIRCONACYCLOBUTANE DERIVATIVE

被引：1
|
作者：
BOHME, U [1 ]
THIELE, KH [1 ]
机构：
[1] TH MERSEBURG,INST ANORGAN CHEM,GEUSAER STR,D-42000 MERSEBURG,GERMANY
来源：
JOURNAL OF ORGANOMETALLIC CHEMISTRY | 1993年 / 452卷 / 1-2期
关键词：
D O I：
10.1016/0022-328X(93)83174-T
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The zirconacyclobutane derivative (tritox)2ZrC(=CH2)CH2CH2 (tritox = (t-C4H9)3CO) with exocyclic methylidine group is formed unexpectedly from (tritox)2ZrCl2 and vinyllithium. The compound was characterized by H-1 and C-13 NMR spectra. The reaction mechanism is discussed. The Zr-91 NMR spectrum of (tritox)2ZrCl2 is reported.
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页码：75 / 78
页数：4
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