SYNTHESIS AND CHARACTERIZATION OF TITANIUM PILLARED CLAYS - INFLUENCE OF THE TEMPERATURE OF PREPARATION

被引：102
作者：
BERNIER, A [1 ]
ADMAIAI, LF [1 ]
GRANGE, P [1 ]
机构：
[1] CATHOLIC UNIV LOUVAIN, UNITE CATALYSE & CHIM MAT DIVISES, PL CROIX SUD 2, BOITE 17, B-1348 LOUVAIN, BELGIUM
来源：
APPLIED CATALYSIS | 1991年 / 77卷 / 02期
关键词：
CATALYST PREPARATION (PILLARING); PILLARED CLAYS; TEMPERATURE EFFECT; TITANIUM;
D O I：
10.1016/0166-9834(91)80071-4
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Detailed analysis of the experimental conditions necessary in order to prepare thermally stable titanium pillared clays are described. pH, temperature and titanium concentration of the suspension play an important role. In the optimal conditions, high surface area Ti PILC (327 m2 g-1 at 600-degrees-C) are prepared. In addition, these microporous materials develop strong Lewis acidity evaluated by TPD of ammonia and FT-IR of pyridine.
引用
收藏
页码：269 / 281
页数：13
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